(E)-3-(2-formylphenyl)-1-phenylallyl acetate

Base Information

Chemical Name:(E)-3-(2-formylphenyl)-1-phenylallyl acetate
CAS No.:1309781-84-7
Molecular Formula:C₁₈H₁₆O₃
Molecular Weight:280.323
Hs Code.:

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Chemical Property of (E)-3-(2-formylphenyl)-1-phenylallyl acetate

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Technology Process of (E)-3-(2-formylphenyl)-1-phenylallyl acetate

There total 5 articles about (E)-3-(2-formylphenyl)-1-phenylallyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1309781-83-6
(E)-3-(2-(1,3-dioxolan-2-yl)phenyl)-1-phenylallyl acetate

: 1309781-84-7
(E)-3-(2-formylphenyl)-1-phenylallyl acetate

Guidance literature:: With hydrogenchloride; ammonium chloride; In water; acetone; for 3h;
DOI:10.1002/anie.201008160

Reference yield:

: 34824-58-3
2-(2-bromophenyl)-1,3-dioxolan

: 1309781-84-7
(E)-3-(2-formylphenyl)-1-phenylallyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: 1,2,2,6,6-pentamethylpiperidine; palladium diacetate; triphenylphosphine / 18 h / 125 °C / Inert atmosphere

2: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0 °C / Inert atmosphere

3: dmap; triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

4: hydrogenchloride; ammonium chloride / water; acetone / 3 h

With 1,2,2,6,6-pentamethylpiperidine; hydrogenchloride; dmap; sodium tetrahydroborate; cerium(III) chloride heptahydrate; palladium diacetate; ammonium chloride; triethylamine; triphenylphosphine; In methanol; dichloromethane; water; acetone;
DOI:10.1002/anie.201008160

Reference yield:

: 1309781-81-4
(E)-3-(2-(1,3-dioxolan-2-yl)phenyl)-1-phenylprop-2-en-1-one

: 1309781-84-7
(E)-3-(2-formylphenyl)-1-phenylallyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0 °C / Inert atmosphere

2: dmap; triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere

3: hydrogenchloride; ammonium chloride / water; acetone / 3 h

With hydrogenchloride; dmap; sodium tetrahydroborate; cerium(III) chloride heptahydrate; ammonium chloride; triethylamine; In methanol; dichloromethane; water; acetone;
DOI:10.1002/anie.201008160