(C₆H₅)2BNC₅H₄C₈H₄NCl

Base Information

• Chemical Name: (C₆H₅)2BNC₅H₄C₈H₄NCl
• CAS No.: 475993-71-6
• Molecular Formula: C₂₅H₁₈BClN₂
• Molecular Weight: 392.695
• Mol file: 475993-71-6.mol

Synonyms:

Chemical Property of (C₆H₅)2BNC₅H₄C₈H₄NCl

Chemical Property:

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Technology Process of (C₆H₅)2BNC₅H₄C₈H₄NCl

There total 1 articles about (C₆H₅)2BNC₅H₄C₈H₄NCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

5-chloro-2-(pyridin-2-yl)-indole (475993-68-1) + triphenylborane (960-71-4) → (C6H5)2BNC5H4C8H4NCl (475993-71-6)

Guidance literature:

In toluene; (N2); refluxing a soln. of boron compd. and ligand in toluene for 6 h; evapn., dissolving in THF/toluene (1:3), standing at room temp. for 2 wk, slow evapn.; elem. anal.;

DOI:10.1021/om020446j

upstream raw materials:

5-chloro-2-(pyridin-2-yl)-indole

triphenylborane