cis-1-ethoxycarbonyl-3-p-nitrophenyl-6,7a-dimethyl-7-oxo-1,4a,7,7a-tetrahydrocyclopent<1,3,4>-oxadiazine

Base Information

Chemical Name:cis-1-ethoxycarbonyl-3-p-nitrophenyl-6,7a-dimethyl-7-oxo-1,4a,7,7a-tetrahydrocyclopent<1,3,4>-oxadiazine
CAS No.:75609-02-8
Molecular Formula:C₂₉H₂₅N₃O₆
Molecular Weight:511.534
Hs Code.:

cis-1-ethoxycarbonyl-3-p-nitrophenyl-6,7a-dimethyl-7-oxo-1,4a,7,7a-tetrahydrocyclopent<e><1,3,4>-oxadiazine

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Chemical Property of cis-1-ethoxycarbonyl-3-p-nitrophenyl-6,7a-dimethyl-7-oxo-1,4a,7,7a-tetrahydrocyclopent<1,3,4>-oxadiazine

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Technology Process of cis-1-ethoxycarbonyl-3-p-nitrophenyl-6,7a-dimethyl-7-oxo-1,4a,7,7a-tetrahydrocyclopent<1,3,4>-oxadiazine

There total 5 articles about cis-1-ethoxycarbonyl-3-p-nitrophenyl-6,7a-dimethyl-7-oxo-1,4a,7,7a-tetrahydrocyclopent<1,3,4>-oxadiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 26307-17-5
2,5-dimethyl-3,4-diphenylcyclopenta-2,4-dienone

: 75609-01-7
ethyl p-nitrobenzoylazocarboxylate

: 75609-02-8
cis-1-ethoxycarbonyl-3-p-nitrophenyl-6,7a-dimethyl-7-oxo-1,4a,7,7a-tetrahydrocyclopent<1,3,4>-oxadiazine

Guidance literature:: In benzene; for 3h; Heating;

Reference yield:

: 75609-04-0
1,2-diphenyl-3,5-dimethyl-4-oxo-6,7-diazabicyclo<3.2.0>hept-2-ene

: 75609-02-8
cis-1-ethoxycarbonyl-3-p-nitrophenyl-6,7a-dimethyl-7-oxo-1,4a,7,7a-tetrahydrocyclopent<1,3,4>-oxadiazine

Guidance literature:: Multi-step reaction with 4 steps

1: 60 percent / pyridine / diethyl ether / 0.5 h

2: H₂ / Pd/C / ethyl acetate / 1 h

3: cyclohexene / 24 h / Heating

4: 85 percent / benzene / 3 h / Heating

With pyridine; hydrogen; cyclohexene; palladium on activated charcoal; In diethyl ether; ethyl acetate; benzene;

Reference yield:

: 75609-03-9
1,2-diphenyl-3,5-dimethyl-6,7-dibenzyloxycarbonyl-4-oxo-6,7-diazabicyclo<3.2.0>hept-2-ene

: 75609-02-8
cis-1-ethoxycarbonyl-3-p-nitrophenyl-6,7a-dimethyl-7-oxo-1,4a,7,7a-tetrahydrocyclopent<1,3,4>-oxadiazine

Guidance literature:: Multi-step reaction with 5 steps

1: 72 percent / H₂ / Pd/C / ethyl acetate / 16 h / Ambient temperature

2: 60 percent / pyridine / diethyl ether / 0.5 h

3: H₂ / Pd/C / ethyl acetate / 1 h

4: cyclohexene / 24 h / Heating

5: 85 percent / benzene / 3 h / Heating

With pyridine; hydrogen; cyclohexene; palladium on activated charcoal; In diethyl ether; ethyl acetate; benzene;