Benzoic acid, 2-(3,4-dichlorophenyl)hydrazide

Base Information

• Chemical Name: Benzoic acid, 2-(3,4-dichlorophenyl)hydrazide
• CAS No.: 13124-03-3
• Molecular Formula: C13H10 Cl2 N2 O
• Molecular Weight: 281.141
• DSSTox Substance ID: DTXSID60156976
• Wikidata: Q83025101

Synonyms:BRN 0665042;BENZOIC ACID, 2-(3,4-DICHLOROPHENYL)HYDRAZIDE;13124-03-3;DTXSID60156976;AKOS000281735;LS-36900;SR-01000398590;SR-01000398590-1

Chemical Property of Benzoic acid, 2-(3,4-dichlorophenyl)hydrazide

Chemical Property:

• XLogP3: 4.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 280.0170183
• Heavy Atom Count: 18
• Complexity: 282

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=O)NNC2=CC(=C(C=C2)Cl)Cl

Technology Process of Benzoic acid, 2-(3,4-dichlorophenyl)hydrazide

There total 2 articles about Benzoic acid, 2-(3,4-dichlorophenyl)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

3,4-dichlorophenylhydrazine hydrochloride (19763-90-7) + benzoyl chloride (98-88-4) → N’-(3,4-dichlorophenyl)benzohydrazide (13124-03-3)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/ol5006449

Reference yield:

→ N’-(3,4-dichlorophenyl)benzohydrazide (13124-03-3)

Guidance literature:

Benzoylchlorid, Bzl., Triaethylamin, 3,4-Dichlor-phenylhydrazin;

DOI:10.1248/yakushi1947.87.1_43

Reference yield: 87.0%

tert-butylisonitrile (119072-55-8,7188-38-7) + N’-(3,4-dichlorophenyl)benzohydrazide (13124-03-3) → (Z)-N-(3-(3,4-dichlorophenyl)-5-phenyl-1,3,4-oxadiazol-2(3H)-ylidene)-2-methylpropan-2-amine (1595319-72-4)

Guidance literature:

With oxygen; palladium diacetate; In toluene; at 80 ℃; for 1h;

DOI:10.1021/ol5006449

upstream raw materials:

3,4-dichlorophenylhydrazine hydrochloride

benzoyl chloride

Downstream raw materials:

(Z)-N-(3-(3,4-dichlorophenyl)-5-phenyl-1,3,4-oxadiazol-2(3H)-ylidene)-2-methylpropan-2-amine

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