Technology Process of C15H16O5
There total 3 articles about C15H16O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran / 0.33 h / -80 °C / Inert atmosphere
1.2: 2 h / -80 - 20 °C / Inert atmosphere
2.1: methanesulfonyl chloride; triethylamine / dichloromethane / Inert atmosphere; Reflux
With
n-butyllithium; methanesulfonyl chloride; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1039/c2ob25299f
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran / 0.33 h / -80 °C / Inert atmosphere
1.2: 2 h / -80 - 20 °C / Inert atmosphere
2.1: methanesulfonyl chloride; triethylamine / dichloromethane / Inert atmosphere; Reflux
With
n-butyllithium; methanesulfonyl chloride; triethylamine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1039/c2ob25299f
- Guidance literature:
-
With
methanesulfonyl chloride; triethylamine;
In
dichloromethane;
optical yield given as %de;
Inert atmosphere;
Reflux;
DOI:10.1039/c2ob25299f