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C31H52O8

Base Information
  • Chemical Name:C31H52O8
  • CAS No.:1422550-02-4
  • Molecular Formula:C31H52O8
  • Molecular Weight:552.749
  • Hs Code.:
C<sub>31</sub>H<sub>52</sub>O<sub>8</sub>

Synonyms:

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Chemical Property of C31H52O8
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Technology Process of C31H52O8

There total 10 articles about C31H52O8 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With Jones reagent; In water; acetone; at -10 ℃;
DOI:10.1016/j.bmcl.2012.10.083
Guidance literature:
Multi-step reaction with 8 steps
1: toluene-4-sulfonic acid / toluene / Reflux
2: Schwartz's reagent; methylmagnesium chloride; copper(l) iodide / tetrahydrofuran / -20 °C
3: pyridinium p-toluenesulfonate / dichloromethane
4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran
5: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 °C
6: sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol
7: acetic acid / tetrahydrofuran / 20 °C
8: Jones reagent / water; acetone / -10 °C
With sodium chlorite; sodium dihydrogenphosphate; copper(l) iodide; Jones reagent; Schwartz's reagent; oxalyl dichloride; tetrabutyl ammonium fluoride; methylmagnesium chloride; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; water; acetone; toluene; tert-butyl alcohol; 5: |Swern Oxidation;
DOI:10.1016/j.bmcl.2012.10.083
Guidance literature:
Multi-step reaction with 7 steps
1: Schwartz's reagent; methylmagnesium chloride; copper(l) iodide / tetrahydrofuran / -20 °C
2: pyridinium p-toluenesulfonate / dichloromethane
3: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran
4: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 °C
5: sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol
6: acetic acid / tetrahydrofuran / 20 °C
7: Jones reagent / water; acetone / -10 °C
With sodium chlorite; sodium dihydrogenphosphate; copper(l) iodide; Jones reagent; Schwartz's reagent; oxalyl dichloride; tetrabutyl ammonium fluoride; methylmagnesium chloride; pyridinium p-toluenesulfonate; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; water; acetone; tert-butyl alcohol; 4: |Swern Oxidation;
DOI:10.1016/j.bmcl.2012.10.083
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