2-Bromo-3-isopropoxypropenal

Base Information

• Chemical Name: 2-Bromo-3-isopropoxypropenal
• CAS No.: 155272-73-4
• Molecular Formula: C6H9BrO2
• Molecular Weight: 193.04
• Mol file: 155272-73-4.mol

Synonyms:2-Bromo-3-isopropoxypropenal;2-bromo-3-isopropoxyacrolein;2-bromo-3-(1-methylethoxy)-2-propenal;

Chemical Property of 2-Bromo-3-isopropoxypropenal

Chemical Property:

• PSA: 26.30000
• LogP: 1.52180

Purity/Quality:

99% ^*data from raw suppliers

2-Bromo-3-isopropoxypropenal 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Bromo-3-isopropoxypropenal

There total 2 articles about 2-Bromo-3-isopropoxypropenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-bromo-3-hydroxypropenal (19263-02-6) + isopropyl alcohol (67-63-0,8013-70-5) → 2-bromo-3-(1-methylethoxy)-2-propenal (155272-73-4)

Guidance literature:

toluene-4-sulfonic acid; In methyl cyclohexane; at 77 - 87 ℃; for 1 - 2h; Heating / reflux;

Reference yield: 81.0%

2-Bromo-malonaldehyde (2065-75-0) + isopropyl alcohol (67-63-0,8013-70-5) → 2-bromo-3-(1-methylethoxy)-2-propenal (155272-73-4)

Guidance literature:

With p-toluenesulfonic acid monohydrate; In water; for 0.5h;

Reference yield: 82.0%

2-bromo-3-(1-methylethoxy)-2-propenal (155272-73-4) + N-{[2'-(2-triphenylmethyl-2H-tetrazol-5-yl)-1,1'-biphenyl-4-yl]methyl}pentaneamidine (918962-64-8) → 2-n-butyl-1-{[2'-(2-triphenylmethyl-2H-tetrazol-5-yl)-1,1'-biphenyl-4-yl]methyl}-1H-imidazole-5-carbaldehyde (171515-67-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 0 - 60 ℃; for 10.5h; Product distribution / selectivity;

upstream raw materials:

2-bromo-3-hydroxypropenal

isopropyl alcohol

2-Bromo-malonaldehyde

Downstream raw materials:

1-(1-Butyl)-2-phenylimidazole-5-carboxaldehyde

7-methyl-6-oxo-5,6,7,8-tetrahydro-imidazo[1,2-a]pyrazine-2-carbaldehyde

7-Methyl-6-oxo-5,6,7,8-tetrahydro-imidazo[1,2-a]pyrazine-3-carbaldehyde

7H-imidazo[1,2-c]thiazole-2-carbaldehyde

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