C₃₇H₃₈ClN₃O₄

Base Information

Chemical Name:C₃₇H₃₈ClN₃O₄
CAS No.:1422344-61-3
Molecular Formula:C₃₇H₃₈ClN₃O₄
Molecular Weight:624.179
Hs Code.:

C<sub>37</sub>H<sub>38</sub>ClN<sub>3</sub>O<sub>4</sub>

Synonyms:

Suppliers and Price of C₃₇H₃₈ClN₃O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₇H₃₈ClN₃O₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₇H₃₈ClN₃O₄

There total 4 articles about C₃₇H₃₈ClN₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5927-18-4
trimethyl phosphonoacetate

: 1422344-59-9
C₃₄H₃₄ClN₃O₃

: 1422344-61-3
C₃₇H₃₈ClN₃O₄

: C₃₇H₃₈ClN₃O₄

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; In acetonitrile; at 20 ℃; for 1h; Overall yield = 91 %; Overall yield = 110 mg;
DOI:10.1021/jo3026059

Reference yield:

: C₃₄H₃₂ClN₃O₄

: 1422344-61-3
C₃₇H₃₈ClN₃O₄

: C₃₇H₃₈ClN₃O₄

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / toluene / 0.5 h / 0 °C / Inert atmosphere

2: N-ethyl-N,N-diisopropylamine; dimethyl sulfoxide; sulfur trioxide pyridine complex / dichloromethane / 0.5 h / 0 °C

3: lithium chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 1 h / 20 °C

With sulfur trioxide pyridine complex; diisobutylaluminium hydride; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; lithium chloride; In dichloromethane; toluene; acetonitrile; 3: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/jo3026059

Reference yield:

: C₃₅H₃₄ClN₃O₄

: 1422344-61-3
C₃₇H₃₈ClN₃O₄

: C₃₇H₃₈ClN₃O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: p-toluenesulfonic acid monohydrate / dichloromethane / 1.5 h / 0 °C

1.3: 19 h / 110 °C

2.1: diisobutylaluminium hydride / toluene / 0.5 h / 0 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine; dimethyl sulfoxide; sulfur trioxide pyridine complex / dichloromethane / 0.5 h / 0 °C

4.1: lithium chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 1 h / 20 °C

With p-toluenesulfonic acid monohydrate; sulfur trioxide pyridine complex; diisobutylaluminium hydride; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; lithium chloride; In dichloromethane; toluene; acetonitrile; 4.1: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1021/jo3026059