Li2[PhB(μ3-N(t)Bu)2]

Base Information

Chemical Name:Li2[PhB(μ3-N(t)Bu)2]
CAS No.:478000-97-4
Molecular Formula:C₂₈H₄₆B₂Li₄N₄
Molecular Weight:488.086
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Li2[PhB(μ3-N(t)Bu)2]

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Technology Process of Li2[PhB(μ3-N(t)Bu)2]

There total 2 articles about Li2[PhB(μ3-N(t)Bu)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 109-72-8,29786-93-4
n-butyllithium

: 10375-18-5
Bis-tert.-butylamino-phenylboran

: 478000-97-4
Li2[PhB(μ3-N(t)Bu)2]

Guidance literature:: In hexane; byproducts: H-n-Bu; (N2); soln. of n-BuLi (2 equiv.) in hexane was added to soln. of B compd. in hexane at -10°C; mixt. was refluxed for 17 h; ppt. allowed to settle; soln. removed via cannula; residue washed (hexane, 0°C);
DOI:10.1139/v02-111

Reference yield:

: 873-51-8
phenylborondichloride

: 478000-97-4
Li2[PhB(μ3-N(t)Bu)2]

Guidance literature:: Multi-step reaction with 2 steps

1: hexane

2: hexane

In hexane;
DOI:10.1139/v02-111

Reference yield: 91.0%

: 478000-97-4
Li2[PhB(μ3-N(t)Bu)2]

: 10026-07-0
tellurium tetrachloride

: 478000-98-5
PhB(μ-N-t-Bu)2TeCl2

Guidance literature:: In toluene; byproducts: Te; (N2); soln. of B compd. (1 equiv.) in toluene was added to soln. of TeCl4 (1 equiv.) in toluene at -78°C; soln. was warmed to room temp.; after 1 h volatiles removed (vac.); residue extd. (CH3CN); filtered; solvent removed (vac.); elem. anal.;
DOI:10.1139/v02-111