2-benzyl-7-methoxy-1-naphthylacetonitrile

Base Information

Chemical Name:2-benzyl-7-methoxy-1-naphthylacetonitrile
CAS No.:360767-03-9
Molecular Formula:C₂₀H₁₇NO
Molecular Weight:287.361
Hs Code.:

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Chemical Property of 2-benzyl-7-methoxy-1-naphthylacetonitrile

Chemical Property:

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Technology Process of 2-benzyl-7-methoxy-1-naphthylacetonitrile

There total 5 articles about 2-benzyl-7-methoxy-1-naphthylacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 41526-55-0
2-phenylmethylene-7-methoxy-1-tetralone

: 360767-03-9
2-benzyl-7-methoxy-1-naphthylacetonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / H₂ / Pd/C / ethyl acetate / 2 h / 20 °C

2: 87 percent / n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

3: DDQ / CH₂Cl₂ / 20 °C

4: 660 mg / TsOH*H₂O / benzene / 1 h / Heating

With n-butyllithium; hydrogen; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In tetrahydrofuran; hexane; dichloromethane; ethyl acetate; benzene;
DOI:10.1081/SCC-100000591

Reference yield:

: 6836-19-7
7-Methoxy-1-tetralone

: 360767-03-9
2-benzyl-7-methoxy-1-naphthylacetonitrile

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / aq. NaOH / ethanol; tetrahydrofuran / 144 h / 20 °C

2: 80 percent / H₂ / Pd/C / ethyl acetate / 2 h / 20 °C

3: 87 percent / n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

4: DDQ / CH₂Cl₂ / 20 °C

5: 660 mg / TsOH*H₂O / benzene / 1 h / Heating

With sodium hydroxide; n-butyllithium; hydrogen; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In tetrahydrofuran; ethanol; hexane; dichloromethane; ethyl acetate; benzene;
DOI:10.1081/SCC-100000591