N₃,1-diphenyl-5-oxo-6-[(1,7-diphenyl-1,5-dihydro-5-oxo-[1,2,4]triazolo[4,3-a]pyrimidin-3-yl)]-1,5-dihydropyrido[2,3-d][1,2,4]triazolo[4,3-a]pyrimidine-3-carboxamide

Base Information

• Chemical Name: N₃,1-diphenyl-5-oxo-6-[(1,7-diphenyl-1,5-dihydro-5-oxo-[1,2,4]triazolo[4,3-a]pyrimidin-3-yl)]-1,5-dihydropyrido[2,3-d][1,2,4]triazolo[4,3-a]pyrimidine-3-carboxamide
• CAS No.: 1309462-44-9
• Molecular Formula: C₃₈H₂₄N₁₀O₃
• Molecular Weight: 668.674

Synonyms:

Chemical Property of N₃,1-diphenyl-5-oxo-6-[(1,7-diphenyl-1,5-dihydro-5-oxo-[1,2,4]triazolo[4,3-a]pyrimidin-3-yl)]-1,5-dihydropyrido[2,3-d][1,2,4]triazolo[4,3-a]pyrimidine-3-carboxamide

Chemical Property:

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MSDS Files:

Useful:

Technology Process of N₃,1-diphenyl-5-oxo-6-[(1,7-diphenyl-1,5-dihydro-5-oxo-[1,2,4]triazolo[4,3-a]pyrimidin-3-yl)]-1,5-dihydropyrido[2,3-d][1,2,4]triazolo[4,3-a]pyrimidine-3-carboxamide

There total 3 articles about N₃,1-diphenyl-5-oxo-6-[(1,7-diphenyl-1,5-dihydro-5-oxo-[1,2,4]triazolo[4,3-a]pyrimidin-3-yl)]-1,5-dihydropyrido[2,3-d][1,2,4]triazolo[4,3-a]pyrimidine-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-[3-(dimethylamino)-2-propenoyl]-1,7-diphenyl-1,5-dihydro-[1,2,4]triazolo[4,3-a]pyrimidin-5-one (1214257-68-7) → N3,1-diphenyl-5-oxo-6-[(1,7-diphenyl-1,5-dihydro-5-oxo-[1,2,4]triazolo[4,3-a]pyrimidin-3-yl)]-1,5-dihydropyrido[2,3-d][1,2,4]triazolo[4,3-a]pyrimidine-3-carboxamide (1309462-44-9)

Guidance literature:

Multi-step reaction with 3 steps

1: acetic acid / 6 h / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

3: triethylamine / 1,4-dioxane / 2 h / Reflux

With potassium carbonate; acetic acid; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

5-[(1,7-diphenyl-1,5-dihydro-5-oxo-[1,2,4]triazolo[4,3-a]pyrimidin-3-yl)]-2-thioxo-2,3-dihydro-1H-pyrido[2,3-d]pyrimidin-4-one (1309462-18-7) → N3,1-diphenyl-5-oxo-6-[(1,7-diphenyl-1,5-dihydro-5-oxo-[1,2,4]triazolo[4,3-a]pyrimidin-3-yl)]-1,5-dihydropyrido[2,3-d][1,2,4]triazolo[4,3-a]pyrimidine-3-carboxamide (1309462-44-9)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: triethylamine / 1,4-dioxane / 2 h / Reflux

With potassium carbonate; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

2-methylsulfanyl-5-[(1,7-diphenyl-1,5-dihydro-5-oxo-[1,2,4]triazolo[4,3-a]pyrimidin-3-yl)]-3H-pyrido[2,3-d]pyrimidin-4-one (1309462-19-8) + 2-anilino-2-oxo-N-phenylethanehydrazonoyl chloride (33101-93-8,132815-67-9) → N3,1-diphenyl-5-oxo-6-[(1,7-diphenyl-1,5-dihydro-5-oxo-[1,2,4]triazolo[4,3-a]pyrimidin-3-yl)]-1,5-dihydropyrido[2,3-d][1,2,4]triazolo[4,3-a]pyrimidine-3-carboxamide (1309462-44-9)

Guidance literature:

With triethylamine; In 1,4-dioxane; for 2h; Reflux;

upstream raw materials:

3-[3-(dimethylamino)-2-propenoyl]-1,7-diphenyl-1,5-dihydro-[1,2,4]triazolo[4,3-a]pyrimidin-5-one

5-[(1,7-diphenyl-1,5-dihydro-5-oxo-[1,2,4]triazolo[4,3-a]pyrimidin-3-yl)]-2-thioxo-2,3-dihydro-1H-pyrido[2,3-d]pyrimidin-4-one

2-methylsulfanyl-5-[(1,7-diphenyl-1,5-dihydro-5-oxo-[1,2,4]triazolo[4,3-a]pyrimidin-3-yl)]-3H-pyrido[2,3-d]pyrimidin-4-one

2-anilino-2-oxo-N-phenylethanehydrazonoyl chloride

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