(1Z)-2-Anilino-2-oxo-N-phenylethanehydrazonoyl chloride

Base Information

• Chemical Name: (1Z)-2-Anilino-2-oxo-N-phenylethanehydrazonoyl chloride
• CAS No.: 33101-93-8
• Molecular Formula: C₁₄H₁₂ClN₃O
• Molecular Weight: 273.722
• Hs Code.: 2928000090
• European Community (EC) Number: 671-397-1
• Mol file: 33101-93-8.mol

Synonyms:2-Oxo-N'-phenyl-2-(phenylamino)acetohydrazonoyl chloride;33101-93-8;(1Z)-2-Anilino-2-oxo-N-phenylethanehydrazonoyl chloride;2-anilino-2-oxo-N-phenylethanehydrazonoyl chloride;PUKSXDOBWDDAGI-AQTBWJFISA-N;AKOS024319032;Acetamide, 2-chloro-2-phenylhydrazono-N-phenyl-;A821623;2-Oxo-N'-phenyl-2-(phenylamino)acetohydrazonoylchloride;2-Oxo-N-phenyl-2-(phenylamino)ethanehydrazonoyl chloride;(1Z)-2-Anilino-2-oxo-N-phenylethanehydrazonoyl chloride #;(1Z)-2-anilino-2-oxo-N-phenyl-ethanehydrazonoyl chloride

Chemical Property of (1Z)-2-Anilino-2-oxo-N-phenylethanehydrazonoyl chloride

Chemical Property:

• Melting Point: 159 °C
• PSA: 53.49000
• Density: 1.23
• LogP: 3.43550
• XLogP3: 4.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 273.0668897
• Heavy Atom Count: 19
• Complexity: 321

Purity/Quality:

97% ^*data from raw suppliers

2-Oxo-N'-phenyl-2-(phenylamino)acetohydrazonoylchloride 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)NC(=O)C(=NNC2=CC=CC=C2)Cl
• Isomeric SMILES: C1=CC=C(C=C1)NC(=O)/C(=N/NC2=CC=CC=C2)/Cl

Technology Process of (1Z)-2-Anilino-2-oxo-N-phenylethanehydrazonoyl chloride

There total 4 articles about (1Z)-2-Anilino-2-oxo-N-phenylethanehydrazonoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-phenylacetoacetamide (102-01-2,98624-45-4) → 2-anilino-2-oxo-N-phenylethanehydrazonoyl chloride (33101-93-8,132815-67-9)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether; sulfuryl chloride

2: alcohol; sodium acetate

With sulfuryl dichloride; diethyl ether; ethanol; sodium acetate;

Reference yield:

2-chloro-N-phenyl-3-oxobutanamide (31844-92-5,119878-78-3) + benzene diazonium chloride (100-34-5) → 2-anilino-2-oxo-N-phenylethanehydrazonoyl chloride (33101-93-8,132815-67-9)

Guidance literature:

With ethanol; sodium acetate;

Reference yield:

ethanol (64-17-5) + 2-chloro-N-phenyl-3-oxobutanamide (31844-92-5,119878-78-3) + sodium acetate (127-09-3) + benzene diazonium chloride (100-34-5) → 2-anilino-2-oxo-N-phenylethanehydrazonoyl chloride (33101-93-8,132815-67-9)

Guidance literature:

upstream raw materials:

ethanol

2-chloro-N-phenyl-3-oxobutanamide

sodium acetate

benzene diazonium chloride

Downstream raw materials:

7-amino-3-phenylcarbamoyl-1-phenyl[1,2,4]triazolo[4,3-a]pyrimidin-5(1H)-one

3-(6-methyl-4-oxo-3H-pyrimidin-2-yl)-4-oxo-4-(4-methylphenyl)-2-(phenylhydrazono)butanilide

3-(6-methyl-4-oxo-3H-pyrimidin-2-yl)-4-oxo-4-phenyl-2-(phenylhydrazono)butanilide