trans,cis-dichlorobis{2-(phenylazo)pyridine}rhenium(III) chloride

Base Information

Chemical Name:trans,cis-dichlorobis{2-(phenylazo)pyridine}rhenium(III) chloride
CAS No.:143280-13-1
Molecular Formula:C₂₂H₁₈Cl₂N₆Re*Cl
Molecular Weight:658.991
Hs Code.:

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Chemical Property of trans,cis-dichlorobis{2-(phenylazo)pyridine}rhenium(III) chloride

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Technology Process of trans,cis-dichlorobis{2-(phenylazo)pyridine}rhenium(III) chloride

There total 1 articles about trans,cis-dichlorobis{2-(phenylazo)pyridine}rhenium(III) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 2569-57-5
2-(phenylazo)pyridine

: 16009-56-6,34387-57-0
acetonitrile(trichloro)bis(triphenylphosphine)-rhenium(III)

: 143280-13-1
trans,cis-dichlorobis{2-(phenylazo)pyridine}rhenium(III) chloride

Guidance literature:: In ethanol; passing a stream of dry N2 through a suspn. of the Re complex in dry ethanol (15 min), addn. of 2-(phenylazo)pyridine, refluxing (8 h) under N2 yielding a deep green soln.; evapg., dissolving the green solid in a min. vol. of CH2Cl2, column chromy. (alumina, CH2Cl2), collection of a deep green band with benzene/acetonitrile (1:1) as eluent, evapg. the green soln., drying (vac., over P4O10); elem. anal.;
DOI:10.1039/DT9920001883