[ReCl₃(CH₃CN)(P(C₆H₅)3)2]

Base Information

Chemical Name:[ReCl₃(CH₃CN)(P(C₆H₅)3)2]
CAS No.:16009-56-6
Molecular Formula:C₃₈H₃₃Cl₃NP₂Re
Molecular Weight:858.2
Hs Code.:

[ReCl<sub>3</sub>(CH<sub>3</sub>CN)(P(C<sub>6</sub>H<sub>5</sub>)3)2]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [ReCl₃(CH₃CN)(P(C₆H₅)3)2]

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Technology Process of [ReCl₃(CH₃CN)(P(C₆H₅)3)2]

There total 2 articles about [ReCl₃(CH₃CN)(P(C₆H₅)3)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 34248-12-9
trichlorooxobis(triphenylphosphine)rhenium(V)

: 13685-61-5
N,N-Bis(trimethylsilyl)aminodiphenylphosphan

: 603-35-0
triphenylphosphine

: 75-05-8,26809-02-9
acetonitrile

: 849371-27-3
[ReCl₂(MeCN)(PPh₃)2(N=C(CH₃)P(O)Ph₂]

: 16009-56-6,34387-57-0
acetonitrile(trichloro)bis(triphenylphosphine)-rhenium(III)

Guidance literature:: In acetonitrile; under N2; a mixt. of Re-contg. compd. (1.20 mmol), Si-contg. compd. (1.20 mmol), and PPh3 (2.64 mmol) in MeCN was heated under reflux for 2 h; the soln. was filtered hot; the complex was washed with MeCN and dried under vac.; the filtrate was left to cool and after 24 h a mixt. of greenand orange crystals was formed;
DOI:10.1039/b417068g