terabutylammonium difluoro(tetraphenylporphyrinato)ferrate(III)

Base Information

• Chemical Name: terabutylammonium difluoro(tetraphenylporphyrinato)ferrate(III)
• CAS No.: 84946-66-7
• Molecular Formula: C₁₆H₃₆N*C₄₄H₂₈F₂FeN₄
• Molecular Weight: 949.045
• Mol file: 84946-66-7.mol

Synonyms:

Chemical Property of terabutylammonium difluoro(tetraphenylporphyrinato)ferrate(III)

Chemical Property:

Purity/Quality:

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Technology Process of terabutylammonium difluoro(tetraphenylporphyrinato)ferrate(III)

There total 1 articles about terabutylammonium difluoro(tetraphenylporphyrinato)ferrate(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

(TPP)FeF (55428-47-2) + tetra-n-butylammoniumfluoride trihydrate (22206-57-1,153005-55-1) → terabutylammonium difluoro(tetraphenylporphyrinato)ferrate(III) (84946-66-7)

Guidance literature:

In dichloromethane; acetonitrile; byproducts: H2O; an excess of Bu4NF*3H2O, the MeCN were added to Fe-complex in CH2Cl2; most of the solvents was removed in a rotating evaporator; crystals filtered, and dried in air; elem. anal.;

DOI:10.1016/S0277-5387(00)81058-X

upstream raw materials:

(TPP)FeF

tetra-n-butylammoniumfluoride trihydrate