Technology Process of C23H23ClFNO
There total 2 articles about C23H23ClFNO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / diethyl ether / 0 °C
2: potassium carbonate; potassium iodide / acetonitrile
With
lithium aluminium tetrahydride; potassium carbonate; potassium iodide;
In
diethyl ether; acetonitrile;
DOI:10.1016/j.bmcl.2012.08.031
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / isopropyl alcohol / Heating
2: ammonium formate; 10% Pd/C / methanol / Heating
3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide
With
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; 10% Pd/C; ammonium formate; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine;
In
methanol; N,N-dimethyl-formamide; isopropyl alcohol;
1: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2012.08.031