C₃₃H₃₉N₇O₇S

Base Information

Chemical Name:C₃₃H₃₉N₇O₇S
CAS No.:1354578-62-3
Molecular Formula:C₃₃H₃₉N₇O₇S
Molecular Weight:677.781
Hs Code.:

C<sub>33</sub>H<sub>39</sub>N<sub>7</sub>O<sub>7</sub>S

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₃₉N₇O₇S

Chemical Property:

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Technology Process of C₃₃H₃₉N₇O₇S

There total 11 articles about C₃₃H₃₉N₇O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1354578-61-2
C₃₃H₃₆N₆O₆S

: 1354578-62-3
C₃₃H₃₉N₇O₇S

Guidance literature:: With hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine; In ethanol; at 20 ℃; for 33.5h; Reflux;
DOI:10.1021/jm2011996

Reference yield:

: 1357450-95-3
Glu(OBzl)-4-cyanobenzylamide*TFA

: 1354578-62-3
C₃₃H₃₉N₇O₇S

Guidance literature:: Multi-step reaction with 4 steps

1.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C / pH 8 - 9

2.1: hydrogen bromide; acetic acid / 3 h / 20 °C

3.1: N,N-dimethyl-formamide / 0.17 h / Cooling with ice

3.2: 0 - 20 °C

4.1: hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / ethanol / 33.5 h / 20 °C / Reflux

With hydroxylamine hydrochloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen bromide; acetic acid; N-ethyl-N,N-diisopropylamine; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm2011996

Reference yield:

: 1221593-80-1
(S)-4-tert-butoxycarbonylamino-4-(4-cyano-benzylcarbamoyl)-butyric acid benzyl ester

: 1354578-62-3
C₃₃H₃₉N₇O₇S

Guidance literature:: Multi-step reaction with 5 steps

1.1: dichloromethane / 1 h / 20 °C

2.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0 - 20 °C / pH 8 - 9

3.1: hydrogen bromide; acetic acid / 3 h / 20 °C

4.1: N,N-dimethyl-formamide / 0.17 h / Cooling with ice

4.2: 0 - 20 °C

5.1: hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / ethanol / 33.5 h / 20 °C / Reflux

With hydroxylamine hydrochloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen bromide; acetic acid; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm2011996