C₂₀H₂₉NO₃

Base Information

Chemical Name:C₂₀H₂₉NO₃
CAS No.:1446490-17-0
Molecular Formula:C₂₀H₂₉NO₃
Molecular Weight:331.455
Hs Code.:

C<sub>20</sub>H<sub>29</sub>NO<sub>3</sub>

Synonyms:

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Chemical Property of C₂₀H₂₉NO₃

Chemical Property:

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Technology Process of C₂₀H₂₉NO₃

There total 5 articles about C₂₀H₂₉NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112-47-0
1,10-Decanediol

: 1446490-17-0
C₂₀H₂₉NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 4 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: pyridinium chlorochromate; silica gel / dichloromethane / 3 h / Inert atmosphere

3.1: titanium(IV) isopropylate; C₂₃H₁₆N₂O₂ / dichloromethane / -40 °C / Inert atmosphere

3.2: 48 h / -40 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / Inert atmosphere; Resolution of racemate

With titanium(IV) isopropylate; C₂₃H₁₆N₂O₂; silica gel; sodium hydride; triethylamine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201300827

Reference yield:

: 100-39-0
benzyl bromide

: 1446490-17-0
C₂₀H₂₉NO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 4 h / 0 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: pyridinium chlorochromate; silica gel / dichloromethane / 3 h / Inert atmosphere

3.1: titanium(IV) isopropylate; C₂₃H₁₆N₂O₂ / dichloromethane / -40 °C / Inert atmosphere

3.2: 48 h / -40 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / Inert atmosphere; Resolution of racemate

With titanium(IV) isopropylate; C₂₃H₁₆N₂O₂; silica gel; sodium hydride; triethylamine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201300827

Reference yield:

: 165960-95-2
10-benzyloxy-1-decanal

: 1446490-17-0
C₂₀H₂₉NO₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: titanium(IV) isopropylate; C₂₃H₁₆N₂O₂ / dichloromethane / -40 °C / Inert atmosphere

1.2: 48 h / -40 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / Inert atmosphere; Resolution of racemate

With titanium(IV) isopropylate; C₂₃H₁₆N₂O₂; triethylamine; In dichloromethane;
DOI:10.1002/chem.201300827