7,10-Bis(4-(diphenylamino)phenyl)-2,3 -dicyanopyrazino phenanthrene

Base Information

• Chemical Name: 7,10-Bis(4-(diphenylamino)phenyl)-2,3 -dicyanopyrazino phenanthrene
• CAS No.: 1803287-94-6
• Molecular Formula: C₅₄H₃₄N₆
• Molecular Weight: 766.904
• Mol file: 1803287-94-6.mol

Synonyms:

Chemical Property of 7,10-Bis(4-(diphenylamino)phenyl)-2,3 -dicyanopyrazino phenanthrene

Chemical Property:

• PKA: -3.52±0.60(Predicted)
• Density: 1.37±0.1 g/cm3(Predicted)

Purity/Quality:

98.5% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7,10-Bis(4-(diphenylamino)phenyl)-2,3 -dicyanopyrazino phenanthrene

There total 2 articles about 7,10-Bis(4-(diphenylamino)phenyl)-2,3 -dicyanopyrazino phenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

7,10-dibromo-2,3-dicyanopyrazinophenanthrene + 4-(diphenylamino)phenyl boronic acid (201802-67-7) → C54H34N6 (1803287-94-6)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; at 80 ℃; for 24h;

DOI:10.1002/anie.201506687

Reference yield: 65.0%

3,6-bis[4-(diphenylamino)phenyl]-9,10-phenanthrenequinone (1415100-79-6) + 2,3-diaminomaleonitrile (18514-52-8) → C54H34N6 (1803287-94-6)

Guidance literature:

With acetic acid; for 12h; Inert atmosphere; Reflux;

DOI:10.1002/anie.202111172

upstream raw materials:

4-(diphenylamino)phenyl boronic acid

3,6-bis[4-(diphenylamino)phenyl]-9,10-phenanthrenequinone

2,3-diaminomaleonitrile