Technology Process of C20H20N6O2
There total 5 articles about C20H20N6O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
acetonitrile;
at 50 - 80 ℃;
Inert atmosphere;
DOI:10.1021/jm301499r
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetic acid / methanol / 49.5 h / 20 - 67 °C / Inert atmosphere
2: tert.-butylnitrite; copper dichloride / dichloromethane; acetonitrile / 1.5 h / 65 °C / Inert atmosphere
3: N-ethyl-N,N-diisopropylamine / acetonitrile / 50 - 80 °C / Inert atmosphere
With
tert.-butylnitrite; acetic acid; N-ethyl-N,N-diisopropylamine; copper dichloride;
In
methanol; dichloromethane; acetonitrile;
2: |Sandmeyer Reaction;
DOI:10.1021/jm301499r
- Guidance literature:
-
Multi-step reaction with 5 steps
1: phenyltrimethylammonium tribromide / tetrahydrofuran / Inert atmosphere
2: tetrahydrofuran / 48 h / 67 °C / Inert atmosphere
3: acetic acid / methanol / 49.5 h / 20 - 67 °C / Inert atmosphere
4: tert.-butylnitrite; copper dichloride / dichloromethane; acetonitrile / 1.5 h / 65 °C / Inert atmosphere
5: N-ethyl-N,N-diisopropylamine / acetonitrile / 50 - 80 °C / Inert atmosphere
With
tert.-butylnitrite; phenyltrimethylammonium tribromide; acetic acid; N-ethyl-N,N-diisopropylamine; copper dichloride;
In
tetrahydrofuran; methanol; dichloromethane; acetonitrile;
4: |Sandmeyer Reaction;
DOI:10.1021/jm301499r
