Technology Process of C35H34N2O3
There total 8 articles about C35H34N2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogenchloride / ethyl acetate / 20 °C
2: hydrogen; palladium on activated charcoal / methanol / 20 °C
With
hydrogenchloride; palladium on activated charcoal; hydrogen;
In
methanol; ethyl acetate;
DOI:10.1016/j.bmcl.2014.01.004
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: N,N-dimethyl-formamide dimethyl acetal / N,N-dimethyl-formamide / 130 °C
1.2: 20 °C
2.1: sodium hydride; potassium iodide / 0 °C / Reflux
3.1: hydrogen; palladium on activated charcoal / ethanol; tetrahydrofuran / 20 °C
4.1: sodium hydride / dichloromethane / 0 - 20 °C
5.1: sodium hydroxide / 1,4-dioxane / 80 °C
6.1: HATU; triethylamine / dichloromethane / 20 °C
7.1: hydrogenchloride / ethyl acetate / 20 °C
8.1: hydrogen; palladium on activated charcoal / methanol / 20 °C
With
hydrogenchloride; palladium on activated charcoal; hydrogen; sodium hydride; N,N-dimethyl-formamide dimethyl acetal; triethylamine; HATU; potassium iodide; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2014.01.004