C₂₈H₃₈F₂N₂O₅Si

Base Information

Chemical Name:C₂₈H₃₈F₂N₂O₅Si
CAS No.:1567326-35-5
Molecular Formula:C₂₈H₃₈F₂N₂O₅Si
Molecular Weight:548.702
Hs Code.:

C<sub>28</sub>H<sub>38</sub>F<sub>2</sub>N<sub>2</sub>O<sub>5</sub>Si

Synonyms:

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Chemical Property of C₂₈H₃₈F₂N₂O₅Si

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Technology Process of C₂₈H₃₈F₂N₂O₅Si

There total 16 articles about C₂₈H₃₈F₂N₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 530-26-7
D-Mannose

: 1567326-35-5
C₂₈H₃₈F₂N₂O₅Si

Guidance literature:: Multi-step reaction with 16 steps

1.1: iodine / 16 h / 20 °C

2.1: sodium cyanide / water / 12 h / 50 °C

2.2: 12 h / 20 °C

3.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

3.2: 20 h / 20 °C

4.1: acetic acid / water / 3.5 h / 50 °C

5.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

6.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

7.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

8.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

9.1: tetrahydrofuran; methanol / 2 h / 20 °C

10.1: potassium carbonate / N,N-dimethyl-formamide

11.1: N-ethyl-N,N-diisopropylamine / dichloromethane

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran

13.1: Dess-Martin periodane / dichloromethane

14.1: diethylamino-sulfur trifluoride / dichloromethane

15.1: hydrogenchloride; methanol / water

16.1: triethylamine; dmap; tert-butyldimethylsilyl chloride / dichloromethane

With pyridine; hydrogenchloride; methanol; dmap; sodium cyanide; trifluoromethylsulfonic anhydride; diethylamino-sulfur trifluoride; tetrabutyl ammonium fluoride; iodine; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; tert-butyldimethylsilyl chloride; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triethyl phosphite; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 7757-38-2,14131-84-1,23262-78-4,27108-13-0,33823-04-0,34685-42-2,57819-52-0,78039-08-4,78039-12-0,78964-16-6,94842-76-9,149342-31-4
2,3:5,6-di-O-isopropylidene-D-mannofuranose

: 1567326-35-5
C₂₈H₃₈F₂N₂O₅Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: sodium cyanide / water / 12 h / 50 °C

1.2: 12 h / 20 °C

2.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

2.2: 20 h / 20 °C

3.1: acetic acid / water / 3.5 h / 50 °C

4.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

5.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

6.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

7.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

8.1: tetrahydrofuran; methanol / 2 h / 20 °C

9.1: potassium carbonate / N,N-dimethyl-formamide

10.1: N-ethyl-N,N-diisopropylamine / dichloromethane

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran

12.1: Dess-Martin periodane / dichloromethane

13.1: diethylamino-sulfur trifluoride / dichloromethane

14.1: hydrogenchloride; methanol / water

15.1: triethylamine; dmap; tert-butyldimethylsilyl chloride / dichloromethane

With pyridine; hydrogenchloride; methanol; dmap; sodium cyanide; trifluoromethylsulfonic anhydride; diethylamino-sulfur trifluoride; tetrabutyl ammonium fluoride; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; tert-butyldimethylsilyl chloride; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triethyl phosphite; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 137126-24-0
(3aR,4R,7S,7aR)-4-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-7-hydroxy-2,2-dimethyltetrahydro-[1,3]-dioxolo-[4,5-c]-pyran-6-one

: 1567326-35-5
C₂₈H₃₈F₂N₂O₅Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.25 h / -30 °C

1.2: 20 h / 20 °C

2.1: acetic acid / water / 3.5 h / 50 °C

3.1: triethylamine; dmap / dichloromethane / 12 h / 20 °C

4.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C

5.1: triethyl phosphite / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

6.1: acetic acid; sodium cyanoborohydride / 0.5 h / 20 °C

7.1: tetrahydrofuran; methanol / 2 h / 20 °C

8.1: potassium carbonate / N,N-dimethyl-formamide

9.1: N-ethyl-N,N-diisopropylamine / dichloromethane

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran

11.1: Dess-Martin periodane / dichloromethane

12.1: diethylamino-sulfur trifluoride / dichloromethane

13.1: hydrogenchloride; methanol / water

14.1: triethylamine; dmap; tert-butyldimethylsilyl chloride / dichloromethane

With pyridine; hydrogenchloride; methanol; dmap; trifluoromethylsulfonic anhydride; diethylamino-sulfur trifluoride; tetrabutyl ammonium fluoride; sodium cyanoborohydride; potassium carbonate; Dess-Martin periodane; tert-butyldimethylsilyl chloride; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triethyl phosphite; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;