[NiCl(C₆Cl₅)(P(CH₃)3)2]

Base Information

Chemical Name:[NiCl(C₆Cl₅)(P(CH₃)3)2]
CAS No.:82647-54-9
Molecular Formula:C₁₂H₁₈Cl₆NiP₂
Molecular Weight:495.63
Hs Code.:

[NiCl(C<sub>6</sub>Cl<sub>5</sub>)(P(CH<sub>3</sub>)3)2]

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [NiCl(C₆Cl₅)(P(CH₃)3)2]

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Technology Process of [NiCl(C₆Cl₅)(P(CH₃)3)2]

There total 1 articles about [NiCl(C₆Cl₅)(P(CH₃)3)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Ni(CClCCl₂)Cl(P(CH₃)3)2

: trans-[Ni(C₆Cl₅)I(PMe₃)2]

: 82647-54-9
[NiCl(C₆Cl₅)(P(CH₃)3)2]

: trans-[Ni(CClCCl₂)I(PMe₃)2]

Guidance literature:: In benzene; room temp., < 5 min; products were not isolated;

Reference yield: 90.0%

: 82647-54-9
[NiCl(C₆Cl₅)(P(CH₃)3)2]

: silver perchlorate

: 75-05-8,26809-02-9
acetonitrile

: trans-[Ni(C₆Cl₅)(PMe₃)2(NCCH₃)]ClO₄

Guidance literature:: In benzene; complex in benzene was added to AgClO4 in benzene, AgCl removed by filtration, to soln. CH3CN was added with stirring; n-hexane was added, ppt. was filtered, dried in vac.; elem. anal.;

Reference yield: 72.0%

: 82647-54-9
[NiCl(C₆Cl₅)(P(CH₃)3)2]

: thallium(I) 2,4-pentanedionate

: 114171-79-8
pentachlorophenyl-2,4-pentanedionate trimethylphosphine nickel(II)

Guidance literature:: In dichloromethane; byproducts: TlCl, P(CH3)3; under N2; a soln. of trans-(NiCl(C6Cl5)(PMe3)2) in CH2Cl2 is added to asuspension of Tl(acac) in CH2Cl2, mixt. is stirred at room temp. for a few min; TlCl so formed is filtered, evapd. in vac. and the residue is treated with EtOH, ppt. is recrystd. from CH2Cl2/EtOH; elem. anal.;
DOI:10.1016/S0020-1693(00)90443-2