CH2CHCH2C(Me)(Ph)(η5-C5H4)titanium trichloride

Base Information

• Chemical Name: CH2CHCH2C(Me)(Ph)(η5-C5H4)titanium trichloride
• CAS No.: 940894-26-8
• Molecular Formula: C₁₆H₁₇Cl₃Ti
• Molecular Weight: 363.55

Synonyms:

Chemical Property of CH2CHCH2C(Me)(Ph)(η5-C5H4)titanium trichloride

Chemical Property:

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Technology Process of CH2CHCH2C(Me)(Ph)(η5-C5H4)titanium trichloride

There total 1 articles about CH2CHCH2C(Me)(Ph)(η5-C5H4)titanium trichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.9%

CH2CHCH2C(CH3)(C6H5)C5H4Si(CH3)3 + titanium tetrachloride (7550-45-0) → CH2CHCH2C(Me)(Ph)(η5-C5H4)titanium trichloride (940894-26-8)

Guidance literature:

In dichloromethane; (Ti:L=9.1:7.7), soln. of TiCl4 in CH2Cl2 treated dropwise with ligand inCH2Cl2, stirred overnight; evapd.(vac.), solidified for 1 d, recrystd.(hexane), elem. anal.;

DOI:10.1016/j.molcata.2006.05.011

upstream raw materials:

titanium tetrachloride

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