C₂₈H₃₁N₃O₂Se

Base Information

Chemical Name:C₂₈H₃₁N₃O₂Se
CAS No.:1559062-42-8
Molecular Formula:C₂₈H₃₁N₃O₂Se
Molecular Weight:520.533
Hs Code.:

C<sub>28</sub>H<sub>31</sub>N<sub>3</sub>O<sub>2</sub>Se

Synonyms:

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Chemical Property of C₂₈H₃₁N₃O₂Se

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Technology Process of C₂₈H₃₁N₃O₂Se

There total 6 articles about C₂₈H₃₁N₃O₂Se which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130-95-0
quinine

: 1559062-42-8
C₂₈H₃₁N₃O₂Se

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / tetrahydrofuran / 0.25 h / 0 °C

1.2: 4 h / 0 - 5 °C

2.1: sodium azide / N,N-dimethyl-formamide / 20 h / 60 °C

3.1: triphenylphosphine / tetrahydrofuran / 4 h / 60 °C

3.2: 10 h / 20 °C

4.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

5.1: potassium tert-butylate; selenium / N,N-dimethyl-formamide / 10 h / 110 °C / Inert atmosphere

6.1: thiophenol / d⁽⁴⁾-methanol

With selenium; sodium azide; potassium tert-butylate; thiophenol; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; d⁽⁴⁾-methanol; N,N-dimethyl-formamide; 3.1: |Staudinger Azide Reduction;
DOI:10.1039/c4ob00027g

Reference yield:

: 249731-47-3
quinine 9O-methanesulfonate

: 1559062-42-8
C₂₈H₃₁N₃O₂Se

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium azide / N,N-dimethyl-formamide / 20 h / 60 °C

2.1: triphenylphosphine / tetrahydrofuran / 4 h / 60 °C

2.2: 10 h / 20 °C

3.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

4.1: potassium tert-butylate; selenium / N,N-dimethyl-formamide / 10 h / 110 °C / Inert atmosphere

5.1: thiophenol / d⁽⁴⁾-methanol

With selenium; sodium azide; potassium tert-butylate; thiophenol; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; d⁽⁴⁾-methanol; N,N-dimethyl-formamide; 2.1: |Staudinger Azide Reduction;
DOI:10.1039/c4ob00027g

Reference yield:

: 1559062-29-1
2-iodo-N-((1S)-(6-methoxyquinolin-4-yl)((2S,4S,5R)-5-vinylquinuclidin-2-yl)methyl)-3-methylbenzamide

: 1559062-42-8
C₂₈H₃₁N₃O₂Se

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate; selenium / N,N-dimethyl-formamide / 10 h / 110 °C / Inert atmosphere

2: thiophenol / d⁽⁴⁾-methanol

With selenium; potassium tert-butylate; thiophenol; In d⁽⁴⁾-methanol; N,N-dimethyl-formamide;
DOI:10.1039/c4ob00027g