3,5-dibromo-quinoline

Base Information

• Chemical Name: 3,5-dibromo-quinoline
• CAS No.: 101861-59-0
• Molecular Formula: C9H5Br2N
• Molecular Weight: 286.95
• Hs Code.: 2933499090
• Mol file: 101861-59-0.mol

Synonyms:3,5-dibromo-quinoline

Chemical Property of 3,5-dibromo-quinoline

Chemical Property:

• Melting Point: 86℃
• Boiling Point: 333.054 °C at 760 mmHg
• Flash Point: 155.226 °C
• PSA: 12.89000
• Density: 1.924 g/cm³
• LogP: 3.75980

Purity/Quality:

98%min ^*data from raw suppliers

3,5-Dibromoquinoline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,5-dibromo-quinoline

There total 7 articles about 3,5-dibromo-quinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

3-bromoquinoline (5332-24-1) → 3,5-dibromoquinoline (101861-59-0)

Guidance literature:

With N-Bromosuccinimide; sulfuric acid; at 0 - 20 ℃; for 1.33333h;

DOI:10.1021/jm400963y

Reference yield:

3-bromoquinolin-5-amine (116632-57-6) → 3,5-dibromoquinoline (101861-59-0)

Guidance literature:

With hydrogen bromide; sodium nitrite; Diazotization_.nachfolgend Behandeln mit Kupferbromuer-Loesung;

Reference yield:

→ 3,5-dibromoquinoline (101861-59-0)

Guidance literature:

at 200 ℃;

upstream raw materials:

3-bromoquinolin-5-amine

3,5-dibromo-[6]quinolylamine

3-bromoquinoline

3-bromo-5-nitroquinoline

Downstream raw materials:

3-methoxy-quinoline-5-carbaldehyde

5-bromo-3-methoxyquinoline

Refernces

• 1、 -. "5-Quinoline derivatives having an anti-bacterial activity". Page/Page column 8. . Retrieved 2010/12/31.
• 2、 -. "ETHANOL OR 1,2-ETHANEDIOL CYCLOHEXYL ANTIBIOTIC DERIVATIVES". Page/Page column 37-38. . Retrieved 2008/06/13.