dineophyltin dihydride

Base Information

Chemical Name:dineophyltin dihydride
CAS No.:1299471-99-0
Molecular Formula:C₂₀H₂₈Sn
Molecular Weight:387.152
Hs Code.:

Synonyms:

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Chemical Property of dineophyltin dihydride

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Technology Process of dineophyltin dihydride

There total 3 articles about dineophyltin dihydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 16853-85-3
lithium aluminium tetrahydride

: 14208-42-5
dineophyltin dichloride

: 1299471-99-0
dineophyltin dihydride

Guidance literature:: In diethyl ether; Et2O soln. of LiAlH4 (0.011 mmol) dropwise added to Et2O soln. of Neoph2SnCl2 (0.0045 mmol) under N2 at room temp., heated at reflux for 3 h; cooled, aq. satd. soln. of NH4Cl added, organic layer separated, dried over Na2SO4, solvent removed under vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2010.12.033

Reference yield: 93.0%

: 16853-85-3
lithium aluminium tetrahydride

: 131025-88-2
bis(2-methyl-2-phenylpropyl)tin dibromide

: 1299471-99-0
dineophyltin dihydride

Guidance literature:: In diethyl ether; Et2O soln. of LiAlH4 (0.011 mmol) dropwise added to Et2O soln. of Neoph2SnBr2 (0.0045 mmol) under N2 at room temp., heated at reflux for 3 h; cooled, aq. satd. soln. of NH4Cl added, organic layer separated, dried over Na2SO4, solvent removed under vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2010.12.033

Reference yield:

: 35293-35-7
2-methyl-2-phenyl-1-propylmagnesium chloride

: 1299471-99-0
dineophyltin dihydride

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: tetrachloromethane

3: diethyl ether

In tetrachloromethane; diethyl ether;
DOI:10.1016/j.jorganchem.2010.12.033