Raceanisodamine

Base Information

Chemical Name:Raceanisodamine
CAS No.:134355-54-7
Molecular Formula:C₁₇H₂₃NO₄
Molecular Weight:305.374
Hs Code.:
Mol file:134355-54-7.mol

Synonyms:RaceAnisodamine

Suppliers and Price of Raceanisodamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Raceanisodamine 95+%
100g
$ 750.00

Crysdot
Raceanisodamine 95+%
10g
$ 150.00

Crysdot
Raceanisodamine 95+%
5g
$ 90.00

Crysdot
Raceanisodamine 95+%
25g
$ 280.00

Chemenu
(1S,3R,5S,6R)-6-hydroxy-8-methyl-8-azabicyclo[3.2.1]octan-3-yl3-hydroxy-2-phenylpropanoate 95%
25g
$ 262.00

Chemenu
(1S,3R,5S,6R)-6-hydroxy-8-methyl-8-azabicyclo[3.2.1]octan-3-yl3-hydroxy-2-phenylpropanoate 95%
100g
$ 701.00

AvaChem
Raceanisodamine
100mg
$ 690.00

AvaChem
Raceanisodamine
10mg
$ 490.00

Total 11 raw suppliers

Chemical Property of Raceanisodamine

Chemical Property:

Appearance/Colour:White powder
Boiling Point:474.6±45.0 °C(Predicted)
PKA:14.12±0.10(Predicted)
PSA：70.00000
Density:1.27±0.1 g/cm3(Predicted)
LogP:1.64160
Storage Temp.:2-8°C

Purity/Quality:

98% ^*data from raw suppliers

Raceanisodamine 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Raceanisodamine

There total 26 articles about Raceanisodamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51-34-3,138-12-5,64069-63-2,124917-17-5
scopolamine

: 17659-49-3,32671-33-3,76831-52-2,85760-60-7,126371-43-5,134355-54-7,138876-55-8,55869-99-3
(-)-Anisodamine

: 126371-43-5
7b-Hydroxyhyoscyamine

: 101-31-5
Hyoscyamine

Guidance literature:: With hydrogen; nickel; In water; at 20 ℃; for 19h;
DOI:10.1016/0031-9422(89)80374-7

Reference yield:

: 6415-90-3,50700-39-5,306-03-6,4607-53-8
(-)-hyoscyamine hydrobromide

: 17659-49-3,32671-33-3,76831-52-2,85760-60-7,126371-43-5,134355-54-7,138876-55-8,55869-99-3
(-)-Anisodamine

Guidance literature:: With α-ketoglutaric acid; Anisodus tanguticus hyoscyamine 6β-hydroxylase; iron(II) sulfate; In various solvent(s); at 30 ℃; for 2h; pH=7.4; Enzyme kinetics;
DOI:10.1055/s-2005-837825

Reference yield:

: (1R,3S,5S)-8-methyl[6β-²H]-8-azabicyclo[3.2.1]octan-3-ol

: C₁₇H₂₂⁽²⁾HNO₄

: 17659-49-3,32671-33-3,76831-52-2,85760-60-7,126371-43-5,134355-54-7,138876-55-8,55869-99-3
(-)-Anisodamine

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; camphor-10-sulfonic acid; dicyclohexyl-carbodiimide / dichloromethane / 72 h / 20 °C

2: hydrogenchloride; water / methanol / 20 °C

3: hyoscyamine 6β-hydroxylase; iron(II) sulfate; α-ketoglutaric acid; sodium L-ascorbate / aq. buffer / 0.5 h / 20 °C / pH 6.9 / Enzymatic reaction

With hydrogenchloride; dmap; α-ketoglutaric acid; camphor-10-sulfonic acid; hyoscyamine 6β-hydroxylase; water; iron(II) sulfate; sodium L-ascorbate; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1021/jacs.8b11585