anhydrosipholenol A 4-o-benzoate

Base Information

• Chemical Name: anhydrosipholenol A 4-o-benzoate
• CAS No.: 1455460-35-1
• Molecular Formula: C₃₇H₅₄O₄
• Molecular Weight: 562.833
• Mol file: 1455460-35-1.mol

Synonyms:

Chemical Property of anhydrosipholenol A 4-o-benzoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of anhydrosipholenol A 4-o-benzoate

There total 2 articles about anhydrosipholenol A 4-o-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.4%

C30H50O3 + benzoic acid anhydride (93-97-0) → anhydrosipholenol A 4-o-benzoate (1455460-35-1)

Guidance literature:

With dmap; In dichloromethane; Reflux;

DOI:10.1002/cmdc.201200516

Reference yield:

sipholenol-A (78518-73-7) → anhydrosipholenol A 4-o-benzoate (1455460-35-1)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / chloroform / 3 h

2: dmap / dichloromethane / Reflux

With dmap; toluene-4-sulfonic acid; In dichloromethane; chloroform;

DOI:10.1002/cmdc.201200516

upstream raw materials:

sipholenol-A

benzoic acid anhydride