5-mesityl-1,9-bis(2,4,6-triphenylphenyl)dipyrrinatocobalt(III) tert-butylimide

Base Information

Chemical Name:5-mesityl-1,9-bis(2,4,6-triphenylphenyl)dipyrrinatocobalt(III) tert-butylimide
CAS No.:1403780-47-1
Molecular Formula:C₇₀H₅₈CoN₃
Molecular Weight:1000.24
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-mesityl-1,9-bis(2,4,6-triphenylphenyl)dipyrrinatocobalt(III) tert-butylimide

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Technology Process of 5-mesityl-1,9-bis(2,4,6-triphenylphenyl)dipyrrinatocobalt(III) tert-butylimide

There total 3 articles about 5-mesityl-1,9-bis(2,4,6-triphenylphenyl)dipyrrinatocobalt(III) tert-butylimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 13686-33-4
t-butyl azide

: 1403780-46-0
5-mesityl-1,9-bis(2,4,6-triphenylphenyl)dipyrrinatocobalt(I) pyridine

: 1403780-47-1
5-mesityl-1,9-bis(2,4,6-triphenylphenyl)dipyrrinatocobalt(III) tert-butylimide

Guidance literature:: In diethyl ether; for 0.416667h;
DOI:10.1021/ja307699u

Reference yield:

: (5-mesityl-1,9-(2,4,6-Ph₃-C₆H₂)dipyrrin)Li

: 1403780-47-1
5-mesityl-1,9-bis(2,4,6-triphenylphenyl)dipyrrinatocobalt(III) tert-butylimide

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / 14 h

2: potassium graphite / benzene / 12 h

3: diethyl ether / 0.42 h

With potassium graphite; In diethyl ether; benzene;
DOI:10.1021/ja307699u

Reference yield:

: 1403780-45-9
5-mesityl-1,9-bis(2,4,6-triphenylphenyl)dipyrrinatocobalt(II) chloride pyridine

: 1403780-47-1
5-mesityl-1,9-bis(2,4,6-triphenylphenyl)dipyrrinatocobalt(III) tert-butylimide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium graphite / benzene / 12 h

2: diethyl ether / 0.42 h

With potassium graphite; In diethyl ether; benzene;
DOI:10.1021/ja307699u