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[Os3(CO)8(μ-SPh)2(μ-bis(diphenylphosphino)methane)]*H2O*H2S

Base Information Edit
  • Chemical Name:[Os3(CO)8(μ-SPh)2(μ-bis(diphenylphosphino)methane)]*H2O*H2S
  • CAS No.:875062-46-7
  • Molecular Formula:C45H32O8Os3P2S2*H2O*H2S
  • Molecular Weight:1449.52
  • Hs Code.:
  • Mol file:875062-46-7.mol
[Os3(CO)8(μ-SPh)2(μ-bis(diphenylphosphino)methane)]*H2O*H2S

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Suppliers and Price of [Os3(CO)8(μ-SPh)2(μ-bis(diphenylphosphino)methane)]*H2O*H2S
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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of [Os3(CO)8(μ-SPh)2(μ-bis(diphenylphosphino)methane)]*H2O*H2S Edit
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Technology Process of [Os3(CO)8(μ-SPh)2(μ-bis(diphenylphosphino)methane)]*H2O*H2S

There total 1 articles about [Os3(CO)8(μ-SPh)2(μ-bis(diphenylphosphino)methane)]*H2O*H2S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In toluene; (N2); std. Schlenk technique; soln. of Os complex and Ph2S2 (2 equiv.) in toluene was refluxed at 110°C for 3 h; solvent removed (vac.); thin-layer chromd. (silica gel, hexane/CH2Cl2, 7/3); recrystd. (hexane/CH2Cl2, -20°C); elem. anal.;
DOI:10.1016/j.jorganchem.2005.08.034
Guidance literature:
In toluene; (N2); std. Schlenk technique; soln. of Os complex in toluene was refluxed for 4 h; solvent removed (vac.); thin-layer chromd. (silica gel, hexane/CH2Cl2, 7/3);
DOI:10.1016/j.jorganchem.2005.08.034
Guidance literature:
In octane; (N2); std. Schlenk technique; soln. of Os complex in octane was refluxedfor 2 h; solvent removed (vac.); thin-layer chromd. (silica gel, hexane/CH2Cl2, 7/3);
DOI:10.1016/j.jorganchem.2005.08.034
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