1-(diphenylphosphinoyl)-1'-([N-(4-pyridyl)methyl]carbamoyl)ferrocene monohydrate

Base Information

• Chemical Name: 1-(diphenylphosphinoyl)-1'-([N-(4-pyridyl)methyl]carbamoyl)ferrocene monohydrate
• CAS No.: 1035458-02-6
• Molecular Formula: C₂₉H₂₅FeN₂O₂P*H₂O
• Molecular Weight: 538.366
• Mol file: 1035458-02-6.mol

Synonyms:

Chemical Property of 1-(diphenylphosphinoyl)-1'-([N-(4-pyridyl)methyl]carbamoyl)ferrocene monohydrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(diphenylphosphinoyl)-1'-([N-(4-pyridyl)methyl]carbamoyl)ferrocene monohydrate

There total 1 articles about 1-(diphenylphosphinoyl)-1'-([N-(4-pyridyl)methyl]carbamoyl)ferrocene monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

1-(diphenylphosphino)-1'-([N-(4-pyridyl)methyl]carbamoyl)ferrocene monohydrate (1035458-09-3) + dihydrogen peroxide (7722-84-1) → 1-(diphenylphosphinoyl)-1'-([N-(4-pyridyl)methyl]carbamoyl)ferrocene monohydrate (1035458-02-6)

Guidance literature:

In acetone; aq. H2O2 was added to a stirred soln. of Fe-cintg. compd. in acetone; stirring for 3.5 h at room temp.; addn. of H2O; acetone was removed under vac. and the aq. residue was extd. with chloroform; the org. layer was dried (MgSO4) and evapd.; column chromy (silicagel, CH2Cl2/MeOH 20:1); crystn. from wet ethyl acetate-hexane; elem. an al.;

DOI:10.1039/b719334c

upstream raw materials:

1-(diphenylphosphino)-1'-([N-(4-pyridyl)methyl]carbamoyl)ferrocene monohydrate

dihydrogen peroxide

Refernces