(E)-3-(3,4-Bis-undecyloxy-phenyl)-acrylic acid 4-{[1-[4-({(E)-4-[(E)-3-(3,4-bis-undecyloxy-phenyl)-acryloyloxy]-phenylimino}-methyl)-phenyl]-meth-(E)-ylidene]-amino}-phenyl ester

Base Information

Chemical Name:(E)-3-(3,4-Bis-undecyloxy-phenyl)-acrylic acid 4-{[1-[4-({(E)-4-[(E)-3-(3,4-bis-undecyloxy-phenyl)-acryloyloxy]-phenylimino}-methyl)-phenyl]-meth-(E)-ylidene]-amino}-phenyl ester
CAS No.:127217-57-6
Molecular Formula:C₈₂H₁₁₆N₂O₈
Molecular Weight:1257.83
Hs Code.:

(E)-3-(3,4-Bis-undecyloxy-phenyl)-acrylic acid 4-{[1-[4-({(E)-4-[(E)-3-(3,4-bis-undecyloxy-phenyl)-acryloyloxy]-phenylimino}-methyl)-phenyl]-meth-(E)-ylidene]-amino}-phenyl ester

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Chemical Property of (E)-3-(3,4-Bis-undecyloxy-phenyl)-acrylic acid 4-{[1-[4-({(E)-4-[(E)-3-(3,4-bis-undecyloxy-phenyl)-acryloyloxy]-phenylimino}-methyl)-phenyl]-meth-(E)-ylidene]-amino}-phenyl ester

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Technology Process of (E)-3-(3,4-Bis-undecyloxy-phenyl)-acrylic acid 4-{[1-[4-({(E)-4-[(E)-3-(3,4-bis-undecyloxy-phenyl)-acryloyloxy]-phenylimino}-methyl)-phenyl]-meth-(E)-ylidene]-amino}-phenyl ester

There total 8 articles about (E)-3-(3,4-Bis-undecyloxy-phenyl)-acrylic acid 4-{[1-[4-({(E)-4-[(E)-3-(3,4-bis-undecyloxy-phenyl)-acryloyloxy]-phenylimino}-methyl)-phenyl]-meth-(E)-ylidene]-amino}-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 693-67-4
bromoundecane

: 127217-57-6
(E)-3-(3,4-Bis-undecyloxy-phenyl)-acrylic acid 4-{[1-[4-({(E)-4-[(E)-3-(3,4-bis-undecyloxy-phenyl)-acryloyloxy]-phenylimino}-methyl)-phenyl]-meth-(E)-ylidene]-amino}-phenyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 75 percent / potassium carbonate / dimethylformamide / 4 h / Heating

2: 92 percent / pyridine, piperidine / ethanol / 20 h / Heating

3: 95 percent / oxalyl chloride / toluene / 1 h / Heating

4: 85 percent / pyridine / 20 h / Ambient temperature

5: tin(II) dichloride dihydrate / ethyl acetate / 7 h / Heating

6: molecular sieves (4 Angstroem) / benzene / 3.5 h / Heating

With piperidine; pyridine; oxalyl dichloride; 4 A molecular sieve; potassium carbonate; tin(ll) chloride; In ethanol; ethyl acetate; N,N-dimethyl-formamide; toluene; benzene;

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 127217-57-6
(E)-3-(3,4-Bis-undecyloxy-phenyl)-acrylic acid 4-{[1-[4-({(E)-4-[(E)-3-(3,4-bis-undecyloxy-phenyl)-acryloyloxy]-phenylimino}-methyl)-phenyl]-meth-(E)-ylidene]-amino}-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / pyridine / 20 h / Ambient temperature

2: tin(II) dichloride dihydrate / ethyl acetate / 7 h / Heating

3: molecular sieves (4 Angstroem) / benzene / 3.5 h / Heating

With pyridine; 4 A molecular sieve; tin(ll) chloride; In ethyl acetate; benzene;

Reference yield:

: 131525-52-5
3,4-Bis-undecyloxy-benzaldehyde

: 127217-57-6
(E)-3-(3,4-Bis-undecyloxy-phenyl)-acrylic acid 4-{[1-[4-({(E)-4-[(E)-3-(3,4-bis-undecyloxy-phenyl)-acryloyloxy]-phenylimino}-methyl)-phenyl]-meth-(E)-ylidene]-amino}-phenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 92 percent / pyridine, piperidine / ethanol / 20 h / Heating

2: 95 percent / oxalyl chloride / toluene / 1 h / Heating

3: 85 percent / pyridine / 20 h / Ambient temperature

4: tin(II) dichloride dihydrate / ethyl acetate / 7 h / Heating

5: molecular sieves (4 Angstroem) / benzene / 3.5 h / Heating

With piperidine; pyridine; oxalyl dichloride; 4 A molecular sieve; tin(ll) chloride; In ethanol; ethyl acetate; toluene; benzene;