benzylsulfonyl-(D)-Ser-Gly-4-cyanaminobenzylamide

Base Information

Chemical Name:benzylsulfonyl-(D)-Ser-Gly-4-cyanaminobenzylamide
CAS No.:1057075-31-6
Molecular Formula:C₂₀H₂₃N₅O₅S
Molecular Weight:445.499
Hs Code.:

Synonyms:

Suppliers and Price of benzylsulfonyl-(D)-Ser-Gly-4-cyanaminobenzylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzylsulfonyl-(D)-Ser-Gly-4-cyanaminobenzylamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzylsulfonyl-(D)-Ser-Gly-4-cyanaminobenzylamide

There total 9 articles about benzylsulfonyl-(D)-Ser-Gly-4-cyanaminobenzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84193-11-3
C₁₄H₁₉N₃O₅

: 1057075-31-6
benzylsulfonyl-(D)-Ser-Gly-4-cyanaminobenzylamide

Guidance literature:: Multi-step reaction with 7 steps

1: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

2: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / DMF (N,N-dimethyl-formamide); dichloromethane / 2.5 h / 20 °C

3: piperazine-1-yl methyl resin; N-ethyl-N,N-diisopropylamine / dichloromethane / 289 h

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 5.5 h / 20 °C

5: hydrogen / palladium on activated charcoal / methanol / 8 h

6: hydrogenchloride / 1,4-dioxane / 7 h / 20 °C

7: sodium acetate / ethanol / 3 h / 20 °C

With hydrogenchloride; piperazine-1-yl methyl resin; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; sodium acetate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane;

Reference yield:

: 18600-42-5
4-nitrobenzylamine hydrochloride

: 1057075-31-6
benzylsulfonyl-(D)-Ser-Gly-4-cyanaminobenzylamide

Guidance literature:: Multi-step reaction with 8 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

2: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

3: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / DMF (N,N-dimethyl-formamide); dichloromethane / 2.5 h / 20 °C

4: piperazine-1-yl methyl resin; N-ethyl-N,N-diisopropylamine / dichloromethane / 289 h

5: N-ethyl-N,N-diisopropylamine / dichloromethane / 5.5 h / 20 °C

6: hydrogen / palladium on activated charcoal / methanol / 8 h

7: hydrogenchloride / 1,4-dioxane / 7 h / 20 °C

8: sodium acetate / ethanol / 3 h / 20 °C

With hydrogenchloride; piperazine-1-yl methyl resin; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; sodium acetate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane;

Reference yield:

: 798560-60-8
Fmoc-(D)-Ser(tBu)-Gly-4-nitrobenzylamide

: 1057075-31-6
benzylsulfonyl-(D)-Ser-Gly-4-cyanaminobenzylamide

Guidance literature:: Multi-step reaction with 5 steps

1: piperazine-1-yl methyl resin; N-ethyl-N,N-diisopropylamine / dichloromethane / 289 h

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 5.5 h / 20 °C

3: hydrogen / palladium on activated charcoal / methanol / 8 h

4: hydrogenchloride / 1,4-dioxane / 7 h / 20 °C

5: sodium acetate / ethanol / 3 h / 20 °C

With hydrogenchloride; piperazine-1-yl methyl resin; hydrogen; sodium acetate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; ethanol; dichloromethane;