H-Gly-4-nitrobenzylamide hydrochloride

Base Information

Chemical Name:H-Gly-4-nitrobenzylamide hydrochloride
CAS No.:84193-63-5
Molecular Formula:C₉H₁₁N₃O₃*ClH
Molecular Weight:245.666
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of H-Gly-4-nitrobenzylamide hydrochloride

Chemical Property:

Purity/Quality:

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Technology Process of H-Gly-4-nitrobenzylamide hydrochloride

There total 1 articles about H-Gly-4-nitrobenzylamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18600-42-5
4-nitrobenzylamine hydrochloride

: 84193-63-5
H-Gly-4-nitrobenzylamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

2: hydrogenchloride / 1,4-dioxane / 1 h / 20 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; dichloromethane;

Reference yield:

: 84193-63-5
H-Gly-4-nitrobenzylamide hydrochloride

: 798560-64-2
benzylsulfonyl-(D)-Ser-Gly-4-aminobenzylamide hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / DMF (N,N-dimethyl-formamide); dichloromethane / 2.5 h / 20 °C

2: piperazine-1-yl methyl resin; N-ethyl-N,N-diisopropylamine / dichloromethane / 289 h

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 5.5 h / 20 °C

4: hydrogen / palladium on activated charcoal / methanol / 8 h

5: hydrogenchloride / 1,4-dioxane / 7 h / 20 °C

With hydrogenchloride; piperazine-1-yl methyl resin; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; DMF (N,N-dimethyl-formamide); dichloromethane;

Reference yield:

: 84193-63-5
H-Gly-4-nitrobenzylamide hydrochloride

: benzylsulfonyl-(D)-Ser-Gly-4-hydroxyguanidinobenzylamide

Guidance literature:: Multi-step reaction with 7 steps

1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / DMF (N,N-dimethyl-formamide); dichloromethane / 2.5 h / 20 °C

2: piperazine-1-yl methyl resin; N-ethyl-N,N-diisopropylamine / dichloromethane / 289 h

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 5.5 h / 20 °C

4: hydrogen / palladium on activated charcoal / methanol / 8 h

5: hydrogenchloride / 1,4-dioxane / 7 h / 20 °C

6: sodium acetate / ethanol / 3 h / 20 °C

7: hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / ethanol / 0 °C

With hydrogenchloride; piperazine-1-yl methyl resin; hydroxylamine hydrochloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; sodium acetate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In 1,4-dioxane; methanol; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane;