C₂₂H₁₅F₂N₃O₄

Base Information

Chemical Name:C₂₂H₁₅F₂N₃O₄
CAS No.:1345868-68-9
Molecular Formula:C₂₂H₁₅F₂N₃O₄
Molecular Weight:423.376
Hs Code.:

C<sub>22</sub>H<sub>15</sub>F<sub>2</sub>N<sub>3</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₁₅F₂N₃O₄

Chemical Property:

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Technology Process of C₂₂H₁₅F₂N₃O₄

There total 6 articles about C₂₂H₁₅F₂N₃O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6628-77-9
6-methoxy-pyridin-3-ylamine

: 1345868-68-9
C₂₂H₁₅F₂N₃O₄

Guidance literature:: Multi-step reaction with 6 steps

1: N,N-dimethyl-formamide / 120 °C

2: diphenylether / Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 120 °C

4: water; potassium hydroxide / ethanol / 20 °C

5: triethylamine; isobutyl chloroformate / dichloromethane / 0 - 20 °C

6: boron tribromide / dichloromethane / Reflux

With diphenylether; water; boron tribromide; potassium carbonate; triethylamine; potassium hydroxide; isobutyl chloroformate; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.09.065

Reference yield:

: 1345868-70-3
C₂₃H₁₇F₂N₃O₄

: 1345868-68-9
C₂₂H₁₅F₂N₃O₄

Guidance literature:: With boron tribromide; In dichloromethane; Reflux;
DOI:10.1016/j.bmcl.2011.09.065

Reference yield:

: 1345869-43-3
C₁₉H₁₆F₂N₂O₄

: 1345868-68-9
C₂₂H₁₅F₂N₃O₄

Guidance literature:: Multi-step reaction with 3 steps

1: water; potassium hydroxide / ethanol / 20 °C

2: triethylamine; isobutyl chloroformate / dichloromethane / 0 - 20 °C

3: boron tribromide / dichloromethane / Reflux

With water; boron tribromide; triethylamine; potassium hydroxide; isobutyl chloroformate; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.09.065