Technology Process of C72H102N5O7(1+)*I(1-)
There total 16 articles about C72H102N5O7(1+)*I(1-) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: trifluoroacetic acid / dichloromethane / 20 °C
2: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 20 °C / Inert atmosphere
3: 24 h / 20 °C
4: tetrakis(actonitrile)copper(I) hexafluorophosphate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / dichloromethane / 20 °C / Inert atmosphere
5: 96 h / 20 °C / Inert atmosphere
With
tetrakis(actonitrile)copper(I) hexafluorophosphate; sodium tris(acetoxy)borohydride; acetic acid; trifluoroacetic acid; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ja501561c
- Guidance literature:
-
Multi-step reaction with 5 steps
1: caesium carbonate; potassium iodide / N,N-dimethyl-formamide / 70 °C
2: sodium tris(acetoxy)borohydride; acetic acid / 1,2-dichloro-ethane / 20 °C / Inert atmosphere
3: 24 h / 20 °C
4: tetrakis(actonitrile)copper(I) hexafluorophosphate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine / dichloromethane / 20 °C / Inert atmosphere
5: 96 h / 20 °C / Inert atmosphere
With
tetrakis(actonitrile)copper(I) hexafluorophosphate; sodium tris(acetoxy)borohydride; caesium carbonate; acetic acid; potassium iodide; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine;
In
dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/ja501561c
