(+/-)--essigsaeure

Base Information

Chemical Name:(+/-)--essigsaeure
CAS No.:30037-06-0
Molecular Formula:C₁₄H₁₇ClO₂S
Molecular Weight:284.807
Hs Code.:

(+/-)-<cis-2-(4-Chlor-phenylmercapto)-cyclohexyl>-essigsaeure

Synonyms:

Suppliers and Price of (+/-)--essigsaeure

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)--essigsaeure

Chemical Property:

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Technology Process of (+/-)--essigsaeure

There total 8 articles about (+/-)--essigsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-54-7
p-Chlorothiophenol

: 30037-06-0,30037-07-1
(+/-)--essigsaeure

Guidance literature:: Multi-step reaction with 4 steps

1: piperidine / 2-methyl-propan-2-ol / Heating

2: HCl / CH₂Cl₂ / 0 °C

3: aq. HCl / Heating

4: (i) LiAlH₄, Et₂O, (ii) SOCl₂, Py, (iii) /BRN= 3587243/, DMSO, (iv) KOH, aq. EtOH

With piperidine; hydrogenchloride; In dichloromethane; tert-butyl alcohol;
DOI:10.1002/hlca.19700530729

Reference yield:

: 18448-47-0
methyl cyclohex-1-ene-1-carboxylate

: 30037-06-0,30037-07-1
(+/-)--essigsaeure

Guidance literature:: Multi-step reaction with 3 steps

1: (i) piperidine, tBuOH, (ii) aq. HCl, (iii) KOH, aq. EtOH

2: LiAlH₄ / diethyl ether / Heating

3: (i) SOCl₂, Py, (ii) /BRN= 3587243/, DMSO, (iii) KOH, aq. EtOH

With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1002/hlca.19700530729

Reference yield:

: 1855-63-6
cyclohex-1-enecarbonitrile

: 30037-06-0,30037-07-1
(+/-)--essigsaeure

Guidance literature:: Multi-step reaction with 4 steps

1: piperidine / 2-methyl-propan-2-ol / Heating

2: HCl / CH₂Cl₂ / 0 °C

3: aq. HCl / Heating

4: (i) LiAlH₄, Et₂O, (ii) SOCl₂, Py, (iii) /BRN= 3587243/, DMSO, (iv) KOH, aq. EtOH

With piperidine; hydrogenchloride; In dichloromethane; tert-butyl alcohol;
DOI:10.1002/hlca.19700530729