cis-1-(n-Hexyl-1-hydroxy-4-phenyl)-3-buten

Base Information

Chemical Name:cis-1-(n-Hexyl-1-hydroxy-4-phenyl)-3-buten
CAS No.:54985-33-0
Molecular Formula:C₁₆H₂₄O
Molecular Weight:232.366
Hs Code.:

Synonyms:

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Chemical Property of cis-1-(n-Hexyl-1-hydroxy-4-phenyl)-3-buten

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Technology Process of cis-1-(n-Hexyl-1-hydroxy-4-phenyl)-3-buten

There total 7 articles about cis-1-(n-Hexyl-1-hydroxy-4-phenyl)-3-buten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2aS*,4S*)-1-phenyldeca-1,2-dien-4-ol

: 54985-33-0
cis-1-(n-Hexyl-1-hydroxy-4-phenyl)-3-buten

: 54985-37-4
trans-1-(n-Hexyl-1-hydroxy-4-phenyl)-3-buten

Guidance literature:: With methanol; bis(pinacol)diborane; copper(l) chloride; sodium t-butanolate; tricyclohexylphosphine; In tetrahydrofuran; at 0 - 25 ℃; for 0.166667h; Overall yield = 61 %; Inert atmosphere;
DOI:10.1002/chem.201705019

Reference yield:

: 536-74-3
phenylacetylene

: 54985-33-0
cis-1-(n-Hexyl-1-hydroxy-4-phenyl)-3-buten

: 54985-37-4
trans-1-(n-Hexyl-1-hydroxy-4-phenyl)-3-buten

Guidance literature:: Multi-step reaction with 4 steps

1: diethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(l) iodide / tetrahydrofuran / 16 h / 20 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid; sodium dihydrogenphosphate / dichloromethane / Inert atmosphere

3: methanol; copper(l) chloride; tricyclohexylphosphine; sodium t-butanolate; bis(pinacol)diborane / tetrahydrofuran / 12 h / 0 - 25 °C / Inert atmosphere; Sealed tube

4: methanol; copper(l) chloride; tricyclohexylphosphine; sodium t-butanolate; bis(pinacol)diborane / tetrahydrofuran / 0.17 h / 0 - 25 °C / Inert atmosphere

With methanol; sodium dihydrogenphosphate; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diethylamine; 3-chloro-benzenecarboperoxoic acid; bis(pinacol)diborane; copper(l) chloride; sodium t-butanolate; tricyclohexylphosphine; In tetrahydrofuran; dichloromethane; 2: |Prilezhaev Epoxydation (mCPBA);
DOI:10.1002/chem.201705019

Reference yield:

: 110792-92-2,110792-97-7
1-[(E)-dec-3-en-1-ynyl]benzene

: 54985-33-0
cis-1-(n-Hexyl-1-hydroxy-4-phenyl)-3-buten

: 54985-37-4
trans-1-(n-Hexyl-1-hydroxy-4-phenyl)-3-buten

Guidance literature:: Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid; sodium dihydrogenphosphate / dichloromethane / Inert atmosphere

2: methanol; copper(l) chloride; tricyclohexylphosphine; sodium t-butanolate; bis(pinacol)diborane / tetrahydrofuran / 12 h / 0 - 25 °C / Inert atmosphere; Sealed tube

3: methanol; copper(l) chloride; tricyclohexylphosphine; sodium t-butanolate; bis(pinacol)diborane / tetrahydrofuran / 0.17 h / 0 - 25 °C / Inert atmosphere

With methanol; sodium dihydrogenphosphate; 3-chloro-benzenecarboperoxoic acid; bis(pinacol)diborane; copper(l) chloride; sodium t-butanolate; tricyclohexylphosphine; In tetrahydrofuran; dichloromethane; 1: |Prilezhaev Epoxydation (mCPBA);
DOI:10.1002/chem.201705019