rac-4¹-<(3-Aminomethyl-phenyl)-methyl>-1,3²-dioxo-2,3,3¹,3²,4,5-hexahydro-2,2,7,8-tetramethyl-pyrrolo<2,3-c>-dipyrrin-9-(10H)-carbonsaeure-tert-butylester

Base Information

• Chemical Name: rac-4¹-<(3-Aminomethyl-phenyl)-methyl>-1,3²-dioxo-2,3,3¹,3²,4,5-hexahydro-2,2,7,8-tetramethyl-pyrrolo<2,3-c>-dipyrrin-9-(10H)-carbonsaeure-tert-butylester
• CAS No.: 129111-96-2
• Molecular Formula: C₂₈H₃₈N₄O₄
• Molecular Weight: 494.634

Synonyms:

Chemical Property of rac-4¹-<(3-Aminomethyl-phenyl)-methyl>-1,3²-dioxo-2,3,3¹,3²,4,5-hexahydro-2,2,7,8-tetramethyl-pyrrolo<2,3-c>-dipyrrin-9-(10H)-carbonsaeure-tert-butylester

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

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Useful:

Technology Process of rac-4¹-<(3-Aminomethyl-phenyl)-methyl>-1,3²-dioxo-2,3,3¹,3²,4,5-hexahydro-2,2,7,8-tetramethyl-pyrrolo<2,3-c>-dipyrrin-9-(10H)-carbonsaeure-tert-butylester

There total 1 articles about rac-4¹-<(3-Aminomethyl-phenyl)-methyl>-1,3²-dioxo-2,3,3¹,3²,4,5-hexahydro-2,2,7,8-tetramethyl-pyrrolo<2,3-c>-dipyrrin-9-(10H)-carbonsaeure-tert-butylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

1,3-di(aminomethyl)benzene (1477-55-0) + (Z)-3,4-dimethyl-5<(4,4-dimethyl-3-methoxycarbonylmethyl-5-oxo-pyrrolydin-2-yliden)methyl>-1H pyrrole-2-carboxylic acid tert-butyl ester (84408-31-1) → rac-41-<(3-Aminomethyl-phenyl)-methyl>-1,32-dioxo-2,3,31,32,4,5-hexahydro-2,2,7,8-tetramethyl-pyrrolo<2,3-c>-dipyrrin-9-(10H)-carbonsaeure-tert-butylester (129111-96-2)

Guidance literature:

In toluene; at 110 ℃; for 4h;

DOI:10.1007/BF00809534

upstream raw materials:

1,3-di(aminomethyl)benzene

(Z)-3,4-dimethyl-5<(4,4-dimethyl-3-methoxycarbonylmethyl-5-oxo-pyrrolydin-2-yliden)methyl>-1H pyrrole-2-carboxylic acid tert-butyl ester

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