1-(4-chlorophenyl)-4-(fluoromethyl)-1H-1,2,3-triazole

Base Information

Chemical Name:1-(4-chlorophenyl)-4-(fluoromethyl)-1H-1,2,3-triazole
CAS No.:1325725-11-8
Molecular Formula:C₉H₇ClFN₃
Molecular Weight:211.626
Hs Code.:

Synonyms:

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Chemical Property of 1-(4-chlorophenyl)-4-(fluoromethyl)-1H-1,2,3-triazole

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Technology Process of 1-(4-chlorophenyl)-4-(fluoromethyl)-1H-1,2,3-triazole

There total 3 articles about 1-(4-chlorophenyl)-4-(fluoromethyl)-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 133902-66-6
1‐(4‐chlorophenyl)‐1H‐1,2,3‐triazole‐4‐yl‐methanol

: 1325725-11-8
1-(4-chlorophenyl)-4-(fluoromethyl)-1H-1,2,3-triazole

Guidance literature:: With dimethylaminosulphur trifluoride; In dichloromethane; at 20 ℃;
DOI:10.1021/jm2003624

Reference yield:

: 3296-05-7
1-azido-4-chlorobenzene

: 1325725-11-8
1-(4-chlorophenyl)-4-(fluoromethyl)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 20 °C / Darkness

2: dimethylaminosulphur trifluoride / dichloromethane / 20 °C

With copper(ll) sulfate pentahydrate; dimethylaminosulphur trifluoride; sodium L-ascorbate; In dichloromethane; water; tert-butyl alcohol; 1: Huisgen cycloaddition;
DOI:10.1021/jm2003624

Reference yield:

: 106-47-8
4-chloro-aniline

: 1325725-11-8
1-(4-chlorophenyl)-4-(fluoromethyl)-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 - 5 °C

1.2: 0 - 20 °C

2.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 20 °C / Darkness

3.1: dimethylaminosulphur trifluoride / dichloromethane / 20 °C

With hydrogenchloride; copper(ll) sulfate pentahydrate; dimethylaminosulphur trifluoride; sodium L-ascorbate; sodium nitrite; In dichloromethane; water; tert-butyl alcohol; 2.1: Huisgen cycloaddition;
DOI:10.1021/jm2003624