N-[(4-Nitrophenyl)methylene]-3-pyridinamine

Base Information

Chemical Name:N-[(4-Nitrophenyl)methylene]-3-pyridinamine
CAS No.:13313-19-4
Molecular Formula:C₁₂H₉N₃O₂
Molecular Weight:227.222
Hs Code.:
DSSTox Substance ID:DTXSID301260498

Synonyms:13313-19-4;DTXSID301260498;AKOS027461565;N-[(4-Nitrophenyl)methylene]-3-pyridinamine

Suppliers and Price of N-[(4-Nitrophenyl)methylene]-3-pyridinamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-[(4-Nitrophenyl)methylene]-3-pyridinamine

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:227.069476538
Heavy Atom Count:17
Complexity:280

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=CN=C1)N=CC2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of N-[(4-Nitrophenyl)methylene]-3-pyridinamine

There total 3 articles about N-[(4-Nitrophenyl)methylene]-3-pyridinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 462-08-8
pyridin-3-ylamine

: 555-16-8
4-nitrobenzaldehdye

: 13313-19-4
(4-nitro-benzylidene)-[3]pyridyl-amine

Guidance literature:: at 100 - 130 ℃;

Reference yield:

: 5918-77-4
2-<(p-nitrobenzylidene)amino>pyridine

: 13313-19-4
(4-nitro-benzylidene)-[3]pyridyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: MCPBA, Na₂CO₃ / CHCl₃ / 5 h / -10 °C

2: 4A molecular sieves / CHCl₃ / 48 h / Ambient temperature

With 4 A molecular sieve; sodium carbonate; 3-chloro-benzenecarboperoxoic acid; In chloroform;