O-[(2,4-Dichlorophenyl)methyl]hydroxylamine

Base Information

Chemical Name:O-[(2,4-Dichlorophenyl)methyl]hydroxylamine
CAS No.:52370-40-8
Molecular Formula:C7H7Cl2NO
Molecular Weight:192.045
Hs Code.:2922199090
Mol file:52370-40-8.mol

Synonyms:2,4–Dichlorobenzylhydroxylamine hydrochloride; 2,4-Dichlorobenzylhydroxylamine; O-(2,4-Dichlorobenzyl)hydroxylamine;

Suppliers and Price of O-[(2,4-Dichlorophenyl)methyl]hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
O-(2,4-Dichlorobenzyl)hydroxylamine 95+%
1g
$ 377.00

Alichem
O-(2,4-Dichlorobenzyl)hydroxylamine
1g
$ 400.00

Total 37 raw suppliers

Chemical Property of O-[(2,4-Dichlorophenyl)methyl]hydroxylamine

Chemical Property:

PSA：35.25000
Density:1.374
LogP:3.08400
Storage Temp.:2-8°C

Purity/Quality:

99% ^*data from raw suppliers

O-(2,4-Dichlorobenzyl)hydroxylamine 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of O-[(2,4-Dichlorophenyl)methyl]hydroxylamine

There total 5 articles about O-[(2,4-Dichlorophenyl)methyl]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.3%

: 339106-00-2
2-(2,4-dichlorobenzyloxy)isoindole-1,3-dione

: 52370-40-8
O-(2,4-dichlorobenzyl)hydroxylamine

Guidance literature:: With hydrazine hydrate; In ethanol; for 1h; Reflux;
DOI:10.1016/j.ejmech.2011.01.031

Reference yield:

: 1777-82-8
(2,4-dichlorophenyl)methanol

: 52370-40-8
O-(2,4-dichlorobenzyl)hydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

2: hydrazine hydrate / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; 1: |Mitsunobu Displacement;
DOI:10.1016/j.ejmech.2015.12.028