bis(pyridine)copper(II) chloride complex

Base Information

Chemical Name:bis(pyridine)copper(II) chloride complex
CAS No.:15092-36-1
Molecular Formula:C₁₀H₁₀Cl₂CuN₂
Molecular Weight:292.655
Hs Code.:

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Chemical Property of bis(pyridine)copper(II) chloride complex

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Technology Process of bis(pyridine)copper(II) chloride complex

There total 4 articles about bis(pyridine)copper(II) chloride complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 6050-13-1
biphenyl-2,2'-dicarboxylic acid anhydride

: Cu₄OCl₆{C₅H₅N}4

: 15092-36-1,13408-58-7,6831-72-7
bis(pyridine)copper(II) chloride complex

: 82762-12-7,76994-01-9
dichloro(diphenato)tetrakis(pyridine)dicopper(II)

Guidance literature:: With pyridine; In dichloromethane; to complex in CH2Cl2 was added C5H5N with stiring, one third of the solvent was pumped off, to the filtrate acid anhydride was added and stirred for 3 h; product was filtered off, washed with ether, dried in vac.;
DOI:10.1039/DT9830001995

Reference yield: 64.0%

: 24457-00-9
4,6-di-tert-butyl-3-nitrocyclohexa-3,5-diene-1,2-dione

: copper(l) chloride

: 15092-36-1,13408-58-7,6831-72-7
bis(pyridine)copper(II) chloride complex

: dichloro(3,5-di-t-butyl-6-nitrocatecholate)tetrakis(pyridine)dicopper(II)

Guidance literature:: With pyridine; In pyridine; a soln. of copper(I) chloride and quinone in pyridine is heated up rapidly (Ar); ppt. (CuCl2(C5H5N)2) is filtered off, washed with ether and dried in vac., elem. anal.; isolation of catecholate complex on evapn. of filtrate to half the vol. and addn. of ether; washing with ether and drying in vac., elem. anal.;
DOI:10.1016/S0020-1693(00)84324-8

Reference yield:

: 24457-00-9
4,6-di-tert-butyl-3-nitrocyclohexa-3,5-diene-1,2-dione

: copper(l) chloride

: 15092-36-1,13408-58-7,6831-72-7
bis(pyridine)copper(II) chloride complex

: dichloro(3,5-di-t-butyl-6-nitrocatecholate)tetrakis(pyridine)dicopper(II)

: dichloro(3,5-di-t-butyl-6-nitrocatecholate)bis(pyridine)copper(II)

Guidance literature:: With pyridine; In pyridine; acetonitrile; to soln. of copper(I) chloride in dry pyridine a soln. of quinone in acetonitrile is added and stirred (Ar); ppt. (CuCl2(C5H5N)2) is filtered off, washed with acetonitrile and dried in vac., elem. anal.; isolation of mixt. of catecholate complexes on evapn. of filtrate to half the vol. and addn. of ether;
DOI:10.1016/S0020-1693(00)84324-8