2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine

Base Information

• Chemical Name: 2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine
• CAS No.: 131088-75-0
• Molecular Formula: C₃₅H₄₇N₃O₁₁
• Molecular Weight: 685.772

Synonyms:

Chemical Property of 2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine

There total 10 articles about 2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2,3-di-O-benzyl-1-N--4,6-O-isopropylidene-β-D-glucopyranosylamine (131088-74-9,131176-17-5) → 2,3-di-O-benzyl-1-N--β-D-glucopyranosylamine (131088-75-0,131176-18-6)

Guidance literature:

With acetic acid; at 40 ℃; for 3h;

DOI:10.1016/0008-6215(90)80006-O

Reference yield: 75.0%

2,3-di-O-benzyl-1-N--4,6-O-isopropylidene-α-D-glucopyranosylamine (131088-74-9,131176-17-5) → 2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine (131088-75-0,131176-18-6)

Guidance literature:

With acetic acid; at 40 ℃; for 3h;

DOI:10.1016/0008-6215(90)80006-O

Reference yield:

2-tert-butoxycarbonylamino-succinic acid 1-benzyl ester (30925-18-9) → 2,3-di-O-benzyl-1-N--β-D-glucopyranosylamine (131088-75-0,131176-18-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 75 percent / triethylamine, diethylcyanophosphonate / CH₂Cl₂; dimethylformamide / 12 h / Ambient temperature

2: 88 percent / H₂ / 10percent Pd-C / ethanol / 12 h / Ambient temperature

3: 41 percent / triethylamine, diethyl cyanophosphonate / tetrahydrofuran / 8 h / Ambient temperature

4: 91 percent / 80percent acetic acid / 3 h / 40 °C

With diethyl cyanophosphonate; hydrogen; acetic acid; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/0008-6215(90)80006-O

upstream raw materials:

2,3-di-O-benzyl-1-N--4,6-O-isopropylidene-β-D-glucopyranosylamine

2-tert-butoxycarbonylamino-succinic acid 1-benzyl ester

L-proline methyl ester monohydrochloride

N-(tert-butoxycarbonyl)-L-aspartyl-L-proline methyl ester

Downstream raw materials:

O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--β-D-glucopyranosylamine

O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine

O-(2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine

O-α-D-glucopyranosyl-(1->6)-O-β-D-glucopyranosyl-(1->6)-2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 131088-75-0 2,3-di-O-benzyl-1-N--α-D-glucopyranosylamine

Send

Send

Metric Ton KG G Pound L ML

Send

Send