2,11-bis(diphenylarsinomethyl)benzophenanthrene

Base Information

Chemical Name:2,11-bis(diphenylarsinomethyl)benzophenanthrene
CAS No.:73850-73-4
Molecular Formula:C₄₄H₃₄As₂
Molecular Weight:712.597
Hs Code.:

2,11-bis(diphenylarsinomethyl)benzo<c>phenanthrene

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,11-bis(diphenylarsinomethyl)benzophenanthrene

Chemical Property:

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Technology Process of 2,11-bis(diphenylarsinomethyl)benzophenanthrene

There total 1 articles about 2,11-bis(diphenylarsinomethyl)benzophenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 61892-30-6
2,11-bis(bromomethyl)benzophenanthrene

: 829-83-4
diphenylarsane

: 73850-73-4
2,11-bis(diphenylarsinomethyl)benzophenanthrene

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) hexane, THF, 0 deg C to RT; 2.) THF, 15 min;
DOI:10.1002/hlca.19800630213

Reference yield: 72.0%

: 15617-18-2,39958-10-6,14220-64-5
bis(benzonitrile)palladium(II) dichloride

: 73850-73-4
2,11-bis(diphenylarsinomethyl)benzophenanthrene

: 73848-88-1
trans-[PdCl₂(2,11-bis(diphenylarsinomethyl)benzo[c]-phenanthrene)]

Guidance literature:: In acetone; under N2, acetone soln. of As compd. was added to stirred soln. of Pd complex in acetone in 1:1 molar ratio, reaction for 12 h; soln. was taken to dryness, residue recrystd. from CH2Cl2/EtOH, dried in vac., elem. anal.;
DOI:10.1002/hlca.19800630213

Reference yield: 70.0%

: 14873-63-3,15617-19-3,51921-56-3
bis(benzonitrile)dichloroplatinum(II)

: 73850-73-4
2,11-bis(diphenylarsinomethyl)benzophenanthrene

: 73848-90-5
trans-[PtCl₂(2,11-bis(diphenylarsinomethyl)benzo[c]-phenanthrene)]

Guidance literature:: In acetone; under N2, acetone soln. of As compd. was added to stirred soln. of Pt complex in acetone in 1:1 molar ratio, reactn. for 12 h; soln. was taken to dryness, residue recrystd. from CH2Cl2/EtOH, dried in vac., elem. anal.;
DOI:10.1002/hlca.19800630213