4-<3-(decyloxy)-4-(3-hydroxypropyl)phenoxy>benzonic acid ethyl ester

Base Information

Chemical Name:4-<3-(decyloxy)-4-(3-hydroxypropyl)phenoxy>benzonic acid ethyl ester
CAS No.:135199-55-2
Molecular Formula:C₂₈H₄₀O₅
Molecular Weight:456.623
Hs Code.:

Synonyms:

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Chemical Property of 4-<3-(decyloxy)-4-(3-hydroxypropyl)phenoxy>benzonic acid ethyl ester

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Technology Process of 4-<3-(decyloxy)-4-(3-hydroxypropyl)phenoxy>benzonic acid ethyl ester

There total 10 articles about 4-<3-(decyloxy)-4-(3-hydroxypropyl)phenoxy>benzonic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 150-19-6
O-methylresorcine

: 135199-55-2
4-<3-(decyloxy)-4-(3-hydroxypropyl)phenoxy>benzonic acid ethyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 36 percent / copper bronze, potassium carbonate / pyridine / 144 h / Heating

2: KOH / ethanol; H₂O / 18 h / Heating

3: 1.) pyridine hydrochloride, 2.) water / 1.) 180-185 deg C, 3 h, 2.) RT, 18 h

4: conc. H₂SO₄ / 48 h / Heating

5: 1.) 60percent NaH / 1.) DMF, mineral oil, RT, 1 h, 2.) DMF, mineral oil, 65 deg C, 18 h

6: 38 percent / 3 h / 200 °C

7: 48 percent / K₂CO₃ / butan-2-one / 96 h / Heating

8: 1.) 0.5 M 9-BBN, 2.) sodium acetate, H₂O₂ / 1.) THF, RT, 19 h, 2.) THF, 1 h

With potassium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; sulfuric acid; water; dihydrogen peroxide; sodium acetate; pyridine hydrochloride; copper; sodium hydride; potassium carbonate; In pyridine; ethanol; water; butanone;
DOI:10.1021/jm00064a006

Reference yield:

: 623-00-7
4-bromobenzenecarbonitrile

: 135199-55-2
4-<3-(decyloxy)-4-(3-hydroxypropyl)phenoxy>benzonic acid ethyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 36 percent / copper bronze, potassium carbonate / pyridine / 144 h / Heating

2: KOH / ethanol; H₂O / 18 h / Heating

3: 1.) pyridine hydrochloride, 2.) water / 1.) 180-185 deg C, 3 h, 2.) RT, 18 h

4: conc. H₂SO₄ / 48 h / Heating

5: 1.) 60percent NaH / 1.) DMF, mineral oil, RT, 1 h, 2.) DMF, mineral oil, 65 deg C, 18 h

6: 38 percent / 3 h / 200 °C

7: 48 percent / K₂CO₃ / butan-2-one / 96 h / Heating

8: 1.) 0.5 M 9-BBN, 2.) sodium acetate, H₂O₂ / 1.) THF, RT, 19 h, 2.) THF, 1 h

With potassium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; sulfuric acid; water; dihydrogen peroxide; sodium acetate; pyridine hydrochloride; copper; sodium hydride; potassium carbonate; In pyridine; ethanol; water; butanone;
DOI:10.1021/jm00064a006

Reference yield:

: 56183-35-8
4-(3-hydroxyphenoxy)benzonic acid

: 135199-55-2
4-<3-(decyloxy)-4-(3-hydroxypropyl)phenoxy>benzonic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: conc. H₂SO₄ / 48 h / Heating

2: 1.) 60percent NaH / 1.) DMF, mineral oil, RT, 1 h, 2.) DMF, mineral oil, 65 deg C, 18 h

3: 38 percent / 3 h / 200 °C

4: 48 percent / K₂CO₃ / butan-2-one / 96 h / Heating

5: 1.) 0.5 M 9-BBN, 2.) sodium acetate, H₂O₂ / 1.) THF, RT, 19 h, 2.) THF, 1 h

With 9-borabicyclo[3.3.1]nonane dimer; sulfuric acid; dihydrogen peroxide; sodium acetate; sodium hydride; potassium carbonate; In butanone;
DOI:10.1021/jm00064a006