Technology Process of benzyl 2<(2R,3S)-2-acetonylsulphonyl-3-chloro-4-oxoazetidin-1-yl>-2-methylbut-2-enoate
There total 5 articles about benzyl 2<(2R,3S)-2-acetonylsulphonyl-3-chloro-4-oxoazetidin-1-yl>-2-methylbut-2-enoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 69 percent / sodium hydrogen carbonate / H2O; ethanol; dimethylformamide / 0.5 h
2: 43 percent / potassium permanganate / H2O; acetic acid / 3.5 h / 0 °C
3: 48 percent / 30percent DBN / CDCl3
4: 1.) sodium hydrogen carbonate, 2.) sodium iodide / 1.) H2O, 0.5 h, 2.) acetone, 24 h
With
potassium permanganate; 2,6-dichloro-benzonitrile; sodium hydrogencarbonate; sodium iodide;
In
chloroform-d1; ethanol; water; acetic acid; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 48 percent / 30percent DBN / CDCl3
2: 1.) sodium hydrogen carbonate, 2.) sodium iodide / 1.) H2O, 0.5 h, 2.) acetone, 24 h
With
2,6-dichloro-benzonitrile; sodium hydrogencarbonate; sodium iodide;
In
chloroform-d1;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 69 percent / sodium hydrogen carbonate / H2O; ethanol; dimethylformamide / 0.5 h
2: 43 percent / potassium permanganate / H2O; acetic acid / 3.5 h / 0 °C
3: 48 percent / 30percent DBN / CDCl3
4: 1.) sodium hydrogen carbonate, 2.) sodium iodide / 1.) H2O, 0.5 h, 2.) acetone, 24 h
With
potassium permanganate; 2,6-dichloro-benzonitrile; sodium hydrogencarbonate; sodium iodide;
In
chloroform-d1; ethanol; water; acetic acid; N,N-dimethyl-formamide;
