p-phenylacetyl chloride hydrochloride

Base Information

• Chemical Name: p-phenylacetyl chloride hydrochloride
• CAS No.: 53039-95-5
• Molecular Formula: C₁₂H₁₄Cl₃NO*ClH
• Molecular Weight: 331.069

Synonyms:

Chemical Property of p-phenylacetyl chloride hydrochloride

Chemical Property:

Purity/Quality:

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Technology Process of p-phenylacetyl chloride hydrochloride

There total 1 articles about p-phenylacetyl chloride hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-bis(2-chloroethyl)aminophenylacetic acid (10477-72-2) → p-phenylacetyl chloride hydrochloride (53039-95-5)

Guidance literature:

With thionyl chloride;

DOI:10.1007/BF00758456

Reference yield: 64.0%

1H-imidazol-5-ylmethanol hydrochloride (32673-41-9) + p-phenylacetyl chloride hydrochloride (53039-95-5) → {4-[bis-(2-chloro-ethyl)-amino]-phenyl}-acetic acid 3H-imidazol-4-ylmethyl ester; compound with GENERIC INORGANIC NEUTRAL COMPONENT

Guidance literature:

at 90 - 100 ℃; for 5h;

DOI:10.1023/A:1010486223184

Reference yield: 50.0%

p-phenylacetyl chloride hydrochloride (53039-95-5) + 2-amino-2-hydroxymethyl-1,3-propanediol (77-86-1) → (2-Hydroxymethyl-1,3-dihydroxy-2-propyl)amide of 4-phenylacetic acid (64205-65-8)

Guidance literature:

In water; acetone; at -10 ℃; for 0.25h;

DOI:10.1007/BF00758456

upstream raw materials:

4-bis(2-chloroethyl)aminophenylacetic acid

Downstream raw materials:

17β-hydroxy-4-aza-5-androsten-3-one p-phenylacetate

17β-hydroxy-3-aza-A-homo-4a-androsten-4-one p-phenylacetate

17β-hydroxy-4-aza-5α-androstan-3-one p-phenylacetate

17β-hydroxy-4-aza-5β-androst-1-en-3-one p-phenylacetate

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