1,1'-ferrocene dicarboxylic anhydride

Base Information

Chemical Name:1,1'-ferrocene dicarboxylic anhydride
CAS No.:12088-92-5
Molecular Formula:C₁₂H₈FeO₃
Molecular Weight:256.041
Hs Code.:

Synonyms:

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Chemical Property of 1,1'-ferrocene dicarboxylic anhydride

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Technology Process of 1,1'-ferrocene dicarboxylic anhydride

There total 2 articles about 1,1'-ferrocene dicarboxylic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1,1'-bisferrocenedicarboxylic acid

: 538-75-0
dicyclohexyl-carbodiimide

: 12088-92-5
1,1'-ferrocene dicarboxylic anhydride

: 107896-08-2
1,1'-bis(1,3-dicyclohexylureidocarbonyl)-ferrocene

Guidance literature:: In ethyl acetate; Sonication; compd. suspended under N2 atm. in EtOAc with sonication then stirred for3 wk at room temp.; residue of carbodiimide decompd. with few drops of HOAc, dissolved in Et2O, extd. with H2O, org. phase evapd., residue recrystd. from EtOAc/n-hexane, chromy. (EtOAc/n-hexane 1/4, silicagel); elem. anal.;
DOI:10.1002/zaac.200400096

Reference yield: 59.0%

: 1,1'-bisferrocenedicarboxylic acid

: 726-42-1
di-p-tolylcarbodiimide

: 12088-92-5
1,1'-ferrocene dicarboxylic anhydride

: 777094-69-6
ferrocene-1,1'-bis(N-p-tolylcarboxamide)

Guidance literature:: In melt; compds. melted under N2 atm.; product dissolved in CH2Cl2, residue of carbodiimide decompd. with few drops of HOAc, Et2O added, extd. with H2O, org. phase evapd., residue recrystd. from EtOAc/n-hexane, chromy. (EtOAc/n-hexane 1/4, silicagel); elem. anal.;
DOI:10.1002/zaac.200400096